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MassMS-NW-9203 2-piperidineethanol C7H15NO (Mass of molecular ion: 129)
Source Temperature: 250 °C Sample Temperature: 150 °C Reservoir, 75 eV
18.0 4.8 27.0 3.1 28.0 7.3 29.0 3.0 30.0 9.3 31.0 2.4 39.0 2.8 41.0 6.1 42.0 6.9 43.0 4.5 44.0 4.5 45.0 1.1 53.0 1.2 54.0 2.8 55.0 6.8 56.0 14.8 57.0 2.6 67.0 1.7 68.0 1.7 69.0 1.0 70.0 2.8 72.0 4.0 82.0 2.5 83.0 1.2 84.0 100.0 85.0 6.2 86.0 1.0 98.0 4.6 100.0 1.0 110.0 1.3 111.0 1.0 128.0 1.6 129.0 1.4
90 MHz in CDCl3
400 MHz in CDCl3
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1H NMR 89.56 MHz C7 H15 N O 0.040 g : 0.5 ml CDCl3 2-piperidineethanol 
Assign. Shift(ppm)
A *1 3.77 B *1 3.75 C 3.32 D 3.02 E 2.74 F 2.60 G 1.84 to 1.19 J 1.59
Hz ppm Int.348.44 3.891 35 343.06 3.831 418 342.38 3.823 401 341.13 3.809 88 340.50 3.802 82 337.00 3.763 895 332.19 3.710 377 330.69 3.693 408 327.94 3.662 32 325.44 3.634 34 319.75 3.571 36 297.63 3.324 1000 282.69 3.157 30 280.38 3.131 68 279.06 3.116 83 277.31 3.097 90 275.00 3.071 55 269.94 3.015 61 267.13 2.983 165 266.75 2.979 165 264.50 2.954 180 257.50 2.876 51 255.31 2.851 39 254.75 2.845 40 251.44 2.808 95 248.50 2.775 85 248.19 2.772 85 247.38 2.763 94 245.19 2.738 179 242.00 2.703 178 239.50 2.675 119 235.13 2.626 147 234.00 2.613 170 232.56 2.597 145 229.56 2.564 62 229.19 2.560 62 226.38 2.528 34 225.13 2.514 37 221.56 2.474 71 220.13 2.458 48 218.56 2.441 57 170.69 1.906 32 169.44 1.892 49 167.81 1.874 63 166.56 1.860 82 163.31 1.824 101 161.69 1.806 136 160.00 1.787 132 157.81 1.763 123 155.00 1.731 85 153.06 1.710 139 149.25 1.667 534 147.13 1.643 218 146.44 1.636 235 143.75 1.606 784 140.44 1.569 329 137.94 1.541 870 136.56 1.525 480 134.56 1.503 334 132.56 1.481 370 131.44 1.468 331 126.69 1.415 219 125.75 1.405 195 125.19 1.398 193 124.19 1.387 174 120.31 1.344 225 118.63 1.325 238 117.50 1.312 207 116.06 1.296 172 113.19 1.264 102 111.00 1.240 128 106.25 1.187 70 102.81 1.148 31 102.38 1.144 33 101.94 1.139 34 100.75 1.125 46 100.31 1.121 43 100.00 1.117 42 96.75 1.081 57
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1H NMR 399.65 MHz C7 H15 N O 0.034 g : 0.5 ml CDCl3 2-piperidineethanol Assign. Shift(ppm)
A *1 3.80 B *1 3.75 C 3.2 D 3.032 E 2.740 F 2.597 G 1.810 J 1.61 K 1.57 L *2 1.42 M *2 1.35 N 1.35 ASSIGNED BY H-H COSY. 90MHZ : HSP-03-798
Hz ppm Int.1532.35 3.835 170 1527.22 3.822 299 1521.48 3.808 478 1516.36 3.795 791 1511.35 3.782 428 1509.03 3.776 454 1503.91 3.764 276 1503.05 3.761 331 1502.44 3.760 425 1502.08 3.759 418 1498.17 3.749 216 1496.70 3.746 465 1493.16 3.737 115 1492.43 3.735 130 1491.09 3.731 178 1485.84 3.718 193 1222.17 3.059 137 1220.09 3.053 196 1218.14 3.049 233 1215.94 3.043 205 1213.87 3.038 137 1209.47 3.027 154 1207.40 3.022 202 1205.44 3.017 279 1203.86 3.013 241 1201.42 3.007 134 1107.79 2.772 109 1105.10 2.766 121 1100.59 2.754 168 1098.39 2.749 146 1096.68 2.745 178 1094.12 2.738 179 1093.26 2.736 172 1089.72 2.727 173 1087.40 2.721 136 1084.84 2.715 131 1082.15 2.708 122 1051.15 2.631 252 1048.34 2.624 235 1038.82 2.600 370 1036.50 2.594 276 1035.77 2.592 285 1026.61 2.569 243 1023.93 2.563 178 732.30 1.833 118 730.35 1.828 151 728.76 1.824 166 727.17 1.820 134 725.22 1.815 130 723.88 1.812 105 721.19 1.805 139 719.12 1.800 145 717.77 1.796 195 715.94 1.792 206 713.01 1.785 132 655.52 1.641 210 652.83 1.634 210 650.63 1.628 122 649.05 1.625 124 645.51 1.616 285 642.70 1.609 439 641.48 1.606 399 640.87 1.604 409 639.89 1.602 409 636.96 1.594 689 631.59 1.581 1000 630.49 1.578 945 625.61 1.566 955 623.17 1.560 369 621.09 1.555 291 618.29 1.548 255 582.15 1.457 181 578.61 1.448 279 574.95 1.439 133 569.46 1.425 206 565.92 1.417 331 562.74 1.409 184 556.88 1.394 136 555.42 1.390 129 554.81 1.389 126 552.98 1.384 246 550.42 1.378 152 548.46 1.373 123 543.33 1.360 173 539.79 1.351 273 535.89 1.341 154 531.37 1.330 124 527.47 1.320 216 523.80 1.311 125 498.29 1.247 125 494.63 1.238 150 487.43 1.220 151 485.72 1.216 204 483.76 1.211 189 481.93 1.206 203 474.61 1.188 172 473.27 1.185 137 470.83 1.179 187
in CDCl3
KBr disc
nujol mull
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