3-苄氧基苯胺

产品名称 3-苄氧基苯胺

CAS号1484-26-0

分子式C13H13NO

分子量199.25

¹³CNMR

Mass

MS-NW-8071          
m-(benzyloxy)aniline
C13H13NO            (Mass of molecular ion:    199)

   Source Temperature: 150 °C
   Sample Temperature: 100 °C
   Direct, 75 eV

      39.0       2.9
      41.0       1.2
      51.0       1.3
      52.0       1.0
      53.0       1.6
      63.0       1.4
      65.0      10.4
      80.0       3.0
      89.0       1.1
      91.0     100.0
      92.0       8.1
      99.5       1.0
     122.0       1.9
     198.0       2.4
     199.0      38.9
     200.0       5.7

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₃ H₁₃ N O	0.055 g : 0.5 ml CDCl₃
m-(benzyloxy)aniline

    Assign.     Shift(ppm)

      A             7.393
      B             7.351
      C             7.294
      D             7.033
      E             6.378
      F             6.281
      G             6.261
      J             4.978
      K             3.51

     Hz     ppm     Int.

   2961.06   7.410    158
   2959.35   7.405    228
   2957.15   7.400     81
   2952.64   7.389    465
   2952.03   7.387    427
   2951.29   7.385    389
   2949.34   7.380     91
   2945.92   7.372    235
   2944.82   7.369    318
   2942.75   7.364     94
   2937.74   7.351    526
   2936.04   7.347    204
   2933.47   7.341     30
   2931.76   7.336    131
   2930.18   7.332    222
   2928.22   7.327     44
   2922.00   7.312    114
   2920.41   7.308    193
   2918.70   7.304    100
   2916.02   7.297     72
   2913.33   7.290    195
   2910.52   7.283     47
   2907.71   7.276     42
   2906.25   7.272     62
   2904.66   7.269     34
   2819.09   7.054    205
   2818.73   7.053    210
   2810.91   7.034    418
   2803.22   7.015    218
   2802.73   7.013    228
   2554.81   6.393    155
   2553.83   6.391    162
   2552.49   6.387    173
   2551.51   6.385    175
   2546.51   6.372    145
   2545.78   6.371    151
   2544.19   6.367    173
   2543.33   6.364    168
   2512.57   6.287    187
   2510.62   6.283    378
   2508.42   6.277    287
   2507.08   6.274    283
   2506.23   6.272    283
   2505.00   6.268    139
   2504.03   6.266    113
   2499.27   6.254    208
   2498.41   6.252    208
   2497.19   6.249    166
   2496.34   6.247    148
   1989.62   4.979   1000
   1402.71   3.510    115

in CDCl3

KBr disc

nujol mull

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