2,2,4-三甲基-1,2-二氢喹啉

Mass

MS-NW-9570          
2,2,4-trimethyl-1,2-dihydroquinoline
C12H15N             (Mass of molecular ion:    173)

   Source Temperature: 250 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      39.0       1.2
      51.0       1.2
      63.0       1.0
      65.0       2.1
      71.5       2.3
      77.0       2.6
      77.5       1.2
      78.5       1.9
      79.0       4.1
      85.5       1.5
      89.0       1.1
      91.0       1.9
     115.0       5.9
     116.0       2.2
     117.0       1.3
     128.0       1.9
     129.0       1.5
     130.0       2.0
     142.0       2.2
     143.0       5.1
     156.0       3.4
     157.0      10.1
     158.0     100.0
     159.0      12.4
     160.0       1.1
     172.0       2.7
     173.0       7.2
     174.0       1.0
     200.0       1.3

Assign. Shift(ppm) A 7.037 B 6.956 C 6.613 D 6.393 E 5.272 F 3.6 G 1.958 J 1.232 ASSIGNED BY C-H COSY. J(E,G)=-1.5HZ

     Hz     ppm     Int.

   2817.14   7.050     87
   2815.67   7.046     91
   2809.57   7.031     92
   2807.98   7.027     99
   2788.82   6.979     52
   2787.48   6.975     50
   2781.37   6.960     83
   2779.91   6.956     78
   2773.68   6.941     63
   2772.22   6.937     58
   2650.76   6.633     77
   2649.54   6.630     79
   2643.31   6.615    112
   2642.09   6.612    112
   2635.74   6.596     64
   2634.64   6.593     64
   2559.57   6.405    102
   2559.20   6.404    106
   2558.35   6.402    105
   2557.98   6.401     96
   2551.64   6.385     96
   2551.27   6.384    102
   2550.42   6.382     96
   2550.05   6.381     89
   2107.91   5.275    131
   2106.57   5.272    130
   2105.22   5.268     58
    783.57   1.961    504
    782.10   1.957    480
    492.55   1.233   1000