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MS-IW-4049 allyl ethyl carbonate C6H10O3 (Mass of molecular ion: 130)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 2.7 19.0 1.1 26.0 3.1 27.0 19.2 28.0 13.4 29.0 74.9 30.0 15.6 31.0 10.3 38.0 1.8 39.0 23.7 40.0 15.1 41.0 82.8 42.0 5.3 43.0 4.3 44.0 3.4 45.0 10.9 55.0 2.2 56.0 1.2 57.0 93.1 58.0 100.0 59.0 5.3 63.0 10.9 84.0 3.3 91.0 2.3 102.0 1.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H10 O3 0.05 ml : 0.5 ml CDCl3 allyl ethyl carbonate Assign. Shift(ppm)
A 5.940 B 5.360 C 5.261 D 4.621 E 4.205 F 1.311
Hz ppm Int.
2394.17 5.991 59 2388.43 5.977 118 2383.67 5.965 71 2382.69 5.962 67 2377.93 5.951 135 2376.95 5.948 79 2372.19 5.936 79 2371.22 5.934 141 2366.46 5.922 81 2365.48 5.919 78 2360.72 5.907 148 2354.98 5.893 78 2152.71 5.387 79 2151.25 5.383 204 2149.66 5.379 216 2148.07 5.375 83 2135.50 5.344 70 2134.03 5.340 179 2132.45 5.336 189 2130.98 5.333 72 2109.74 5.279 89 2108.52 5.276 213 2107.30 5.273 201 2105.96 5.270 81 2099.37 5.254 80 2098.02 5.250 192 2096.80 5.247 190 2095.46 5.244 79 1851.32 4.633 287 1849.98 4.630 401 1848.51 4.626 275 1845.58 4.618 277 1844.24 4.615 395 1842.77 4.611 277 1691.53 4.233 232 1684.45 4.215 607 1677.25 4.197 619 1670.17 4.180 260 531.25 1.330 636 528.56 1.323 41 524.05 1.312 1000 521.36 1.305 80 516.97 1.294 630 514.28 1.287 50
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