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网站主页CAS数据库列表 1459-55-8更多图谱4-(1-金刚烷基)甲苯(1459-55-8)核磁图(1HNMR)

4-(1-金刚烷基)甲苯

产品名称 4-(1-金刚烷基)甲苯

CAS号1459-55-8

分子式C17H22

分子量226.36

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  • Mass

    MS-IW-9280          
    1-(p-tolyl)adamantane
    C17H22              (Mass of molecular ion:    226)
    

       Source Temperature: 140 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          27.0       1.5
          29.0       1.3
          39.0       2.9
          41.0       5.7
          51.0       1.5
          53.0       2.2
          55.0       1.8
          65.0       3.0
          67.0       2.2
          77.0       6.5
          78.0       2.4
          79.0       7.5
          80.0       1.0
          81.0       1.1
          84.0       1.1
          89.0       1.3
          90.0       1.3
          91.0      10.8
          92.0       3.8
          93.0       3.5
          94.0      10.2
          95.0       1.5
         103.0       1.2
         105.0      13.7
         106.0       1.8
         115.0       5.9
         116.0       2.2
         117.0       3.8
         118.0       1.5
         119.0       2.2
         121.0       2.2
         127.0       1.5
         128.0       4.9
         129.0       4.2
         130.0       1.0
         131.0       2.1
         132.0      23.1
         133.0       5.2
         134.0       2.0
         141.0       3.7
         142.0       2.4
         143.0       2.5
         152.0       1.9
         153.0       3.3
         154.0       6.4
         155.0       4.5
         156.0       2.9
         157.0       3.4
         165.0       1.1
         167.0       2.4
         168.0       4.0
         169.0     100.0
         170.0      19.0
         171.0       2.2
         183.0      10.0
         184.0       2.8
         211.0       1.5
         226.0      73.9
         227.0      13.8
         228.0       1.2
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C17 H22 0.040 g : 0.5 ml CDCl3
    1-(p-tolyl)adamantane
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.254 B 7.128 C 2.313 D 2.080 E 1.898 F *1 1.77 G *1 1.75

         Hz     ppm     Int.
    

       2906.49   7.273     52
       2904.05   7.267    285
       2902.22   7.262    106
       2897.71   7.251    126
       2895.75   7.246    400
       2893.55   7.241     69
       2852.66   7.138    281
       2852.05   7.137    301
       2844.12   7.117    238
       2843.51   7.116    195
        924.68   2.314   1000
        831.30   2.081    236
        760.01   1.902    798
        757.20   1.895    744
        718.51   1.798     78
        706.30   1.768    303
        703.00   1.760    317
        701.29   1.755    284
        700.07   1.752    317
        690.92   1.729     60
        688.11   1.722     81
    

in CDCl3



KBr disc



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