-
MassMS-NW-9035 (+)-ammonium 3-bromo-8-camphorsulfonate C10H18BrNO4S (Mass of molecular ion: 327)
Source Temperature: 210 °C Sample Temperature: 210 °C Direct, 75 eV
16.0 2.8 17.0 3.5 18.0 1.0 27.0 4.6 29.0 3.1 39.0 11.2 40.0 3.2 41.0 14.6 42.0 1.2 43.0 5.7 51.0 3.3 52.0 1.8 53.0 8.0 54.0 1.8 55.0 7.5 63.0 1.1 64.0 1.0 65.0 6.5 66.0 2.3 67.0 9.9 68.0 15.7 69.0 14.0 77.0 11.7 78.0 3.1 79.0 23.3 80.0 7.3 81.0 30.4 82.0 6.8 83.0 1.9 91.0 17.1 92.0 3.4 93.0 32.7 94.0 8.3 95.0 6.1 96.0 1.4 99.0 7.0 103.0 1.5 105.0 12.6 106.0 6.5 107.0 30.9 108.0 5.2 109.0 3.7 119.0 4.1 120.0 2.8 121.0 100.0 122.0 13.6 123.0 3.1 131.0 3.2 133.0 1.3 135.0 12.5 136.0 1.8 145.0 1.0 147.0 1.0 148.0 1.7 149.0 30.7 150.0 5.3 151.0 2.2 159.0 2.2 161.0 1.7 163.0 4.3 167.0 7.1 175.0 1.6 185.0 1.6 187.0 2.2 188.0 3.8 189.0 1.8 190.0 1.0 200.0 8.6 201.0 5.3 202.0 12.2 203.0 20.7 204.0 2.4 213.0 5.8 229.0 2.0 230.0 2.0 231.0 27.4 232.0 4.1 233.0 1.6 310.0 8.9 311.0 1.2 312.0 9.3 313.0 1.2
400 MHz in DMSO-d6
-
1H NMR 399.65 MHz C10 H18 Br N O4 S 0.038 g : 0.5 ml DMSO-d6 (+)-ammonium 3-bromo-8-camphorsulfonate 
Assign. Shift(ppm)
A 7.17 B 4.992 C 2.995 D *1 2.875 E *1 2.436 F *2 2.141 G *2 1.846 J *3 1.752 K *3 1.187 L 1.097 M 0.830 assigned by C-H COSY
Hz ppm Int.2867.31 7.175 443 1998.41 5.001 85 1997.56 4.999 88 1993.53 4.989 87 1992.80 4.987 86 1201.54 3.007 61 1197.14 2.996 103 1192.87 2.985 61 1154.17 2.888 88 1140.14 2.853 102 980.35 2.454 162 966.31 2.418 141 847.29 2.121 35 747.56 1.871 34 747.31 1.870 34 741.58 1.856 36 738.04 1.847 56 734.25 1.838 32 724.98 1.815 30 700.32 1.753 45 489.14 1.224 30 483.64 1.211 33 479.61 1.201 36 474.61 1.188 50 469.73 1.176 34 438.72 1.098 734 332.03 0.831 1000
in DMSO-d6
KBr disc
nujol mull
更多供应商
