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MassMS-NW-6617 ethyl oxanilate C10H11NO3 (Mass of molecular ion: 193)
Source Temperature: 240 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.0 18.0 1.7 26.0 1.8 27.0 9.6 28.0 3.8 29.0 42.4 30.0 1.2 31.0 1.7 37.0 1.1 38.0 2.6 39.0 8.9 40.0 1.5 41.0 1.2 44.0 3.2 45.0 2.3 50.0 3.6 51.0 11.1 52.0 2.2 62.0 1.0 63.0 3.3 64.0 4.5 65.0 14.2 66.0 6.2 76.0 3.1 77.0 48.0 78.0 4.2 79.0 1.4 91.0 5.5 92.0 33.5 93.0 22.1 94.0 2.2 103.0 4.3 106.0 8.3 107.0 1.0 119.0 27.8 120.0 100.0 121.0 13.7 122.0 1.1 193.0 67.6 194.0 8.3 195.0 1.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C10 H11 N O3 0.046 g : 0.5 ml CDCl3 ethyl oxanilate 
Assign. Shift(ppm)
A 8.9 B 7.64 C 7.37 D 7.16 E 4.393 F 1.407 J(E,F)=7.1HZ.
Hz ppm Int.690.44 7.710 94 688.81 7.692 146 686.63 7.667 45 683.50 7.632 93 681.63 7.611 218 680.44 7.598 228 668.25 7.462 66 666.31 7.440 85 664.31 7.418 38 662.44 7.397 35 659.75 7.367 233 658.00 7.348 71 657.13 7.338 45 653.69 7.299 68 652.06 7.281 142 650.81 7.267 110 649.63 7.254 99 648.00 7.236 178 646.44 7.218 89 643.94 7.191 46 641.00 7.158 92 640.25 7.149 31 634.00 7.080 34 404.63 4.518 109 397.31 4.437 421 390.19 4.357 447 383.19 4.279 132 133.00 1.486 448 125.94 1.407 1000 118.75 1.326 395
in CDCl3
KBr disc
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