图谱信息 供应商 相关产品
网站主页CAS数据库列表 14495-51-3更多图谱2-溴-5-氯甲苯(14495-51-3)Raman光谱

2-溴-5-氯甲苯

产品名称 2-溴-5-氯甲苯

CAS号14495-51-3

分子式C7H6BrCl

分子量205.48

展开


  • Mass

    MS-IW-2209          
    2-bromo-5-chlorotoluene
    C7H6BrCl            (Mass of molecular ion:    204)
    

       Source Temperature: 220 °C
       Sample Temperature: 160 °C
       Reservoir, 75 eV
    

          37.0       2.4
          38.0       3.8
          39.0      10.4
          43.0       3.8
          43.5       1.0
          44.0      10.3
          44.5       2.4
          49.0       2.0
          50.0       6.0
          51.0       5.5
          60.0       1.0
          61.0       5.1
          62.0      13.6
          62.5       1.8
          63.0      26.3
          64.0       4.5
          65.0       1.9
          73.0       6.1
          74.0       4.1
          75.0       4.7
          84.0       5.6
          85.0       6.6
          86.0       4.1
          87.0       3.9
          88.0       2.0
          89.0      56.2
          90.0      16.6
          91.0       1.2
          97.0       1.5
          99.0       8.1
         101.0       2.4
         102.0       1.4
         103.0       1.7
         123.0       2.7
         124.0      11.6
         125.0      85.3
         126.0      10.1
         127.0      27.2
         128.0       2.1
         169.0      26.9
         170.0       2.2
         171.0      26.1
         172.0       2.0
         203.0       3.8
         204.0      77.2
         205.0      10.7
         206.0     100.0
         207.0       8.8
         208.0      24.1
         209.0       1.8
    

400 MHz in CDCl3

parameter in CS2


  • 1H NMR 399.65 MHz
    C7 H6 Br Cl 0.05 ml : 0.5 ml CDCl3
    2-bromo-5-chlorotoluene
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.378 B 7.159 C 6.975 D 2.321

         Hz     ppm     Int.
    

       2953.13   7.390    306
       2944.70   7.369    336
       2862.79   7.164    212
       2862.30   7.163    232
       2860.11   7.157    226
       2859.74   7.156    244
       2793.58   6.991    148
       2792.97   6.989    164
       2791.63   6.986     76
       2791.02   6.984    142
       2790.41   6.983    155
       2785.03   6.969    128
       2784.55   6.968    144
       2782.47   6.963    128
       2781.86   6.961    138
        927.49   2.321   1000
    


  • 1H NMR 300 MHz
    C7 H6 Br Cl 10 mol% in CS2
    2-bromo-5-chlorotoluene
    ChemicalStructure
        Parameter     ppm  Hz
    D(A) 7.097 D(B) 6.919 D(C) 7.317 D(D) 2.313 J(A,B) 2.55 J(A,C) 0.33 J(A,D) -0.63 J(B,C) 8.48 J(B,D) -0.58 J(C,D) 0.40 KOTOWYCZ,G. & SCHAEFER,T. CAN.J.CHEM. 44, 2743 (1966)

         Hz     ppm     Int.
    

       2199.50   7.332    178
       2191.04   7.303    208
       2130.40   7.101    153
       2127.97   7.093    165
       2081.26   6.938     94
       2080.84   6.936     96
       2078.78   6.929     86
       2078.22   6.927     85
       2072.80   6.909     83
       2072.38   6.908     83
       2070.32   6.901     75
       2069.81   6.899     73
        693.82   2.313   1000
    

in CDCl3



liquid film