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MassMS-NW-6218 chloro(p-methoxyphenyl)diphenylmethane C20H17ClO (Mass of molecular ion: 308)
Source Temperature: 170 °C Sample Temperature: 120 °C Direct, 75 eV
15.0 1.2 18.0 1.6 36.0 1.3 39.0 1.5 50.0 1.3 51.0 3.0 63.0 1.8 75.0 1.2 76.0 1.4 77.0 7.2 78.0 1.1 88.0 1.4 89.0 1.0 91.0 1.0 94.5 1.1 100.0 1.3 101.0 3.8 102.0 1.1 105.0 9.0 106.0 1.1 107.0 1.0 107.5 1.1 108.0 1.1 113.0 3.2 113.5 1.0 114.0 2.2 115.0 2.2 119.5 1.5 120.0 1.3 126.0 1.2 128.0 1.3 129.0 1.0 135.0 4.9 136.0 1.6 136.5 2.0 139.0 1.2 151.0 1.7 152.0 6.1 153.0 3.2 163.0 1.1 165.0 12.9 166.0 2.5 180.0 2.0 181.0 2.2 185.0 1.7 189.0 1.5 195.0 8.7 196.0 1.9 197.0 2.9 200.0 1.1 201.0 1.2 202.0 5.6 203.0 2.6 213.0 15.4 214.0 2.8 215.0 7.0 216.0 1.5 226.0 4.9 227.0 3.8 228.0 8.9 229.0 12.4 230.0 3.9 239.0 2.4 240.0 1.2 241.0 4.2 242.0 1.7 243.0 1.5 257.0 2.6 258.0 8.7 259.0 1.9 271.0 2.3 272.0 3.3 273.0 100.0 274.0 25.6 275.0 3.7 290.0 6.9 291.0 1.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C20 H17 Cl O 0.049 g : 0.5 ml CDCl3 chloro(p-methoxyphenyl)diphenylmethane 
Assign. Shift(ppm)
A 7.27 B 7.15 C 6.811 D 3.782
Hz ppm Int.650.69 7.266 1000 645.31 7.206 39 644.63 7.198 78 642.31 7.172 27 637.81 7.122 31 635.44 7.096 118 613.19 6.847 116 610.81 6.821 27 604.06 6.745 59 338.69 3.782 448
in CDCl3
KBr disc
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