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网站主页CAS数据库列表 1444-65-1更多图谱2-苯基环已酮(1444-65-1)Raman光谱

2-苯基环已酮

产品名称 2-苯基环已酮

CAS号1444-65-1

分子式C12H14O

分子量174.24

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  • Mass

    MS-NW-6741          
    2-phenylcyclohexanone
    C12H14O             (Mass of molecular ion:    174)
    

       Source Temperature: 180 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          27.0       4.7
          28.0       1.0
          29.0       1.4
          39.0       8.8
          40.0       1.1
          41.0       4.5
          42.0       2.6
          50.0       2.9
          51.0       7.6
          52.0       2.1
          53.0       1.4
          55.0       4.2
          62.0       1.3
          63.0       4.5
          64.0       1.7
          65.0       5.1
          67.0       1.7
          68.0       2.5
          74.0       1.0
          75.0       1.1
          76.0       1.3
          77.0      10.5
          78.0       9.0
          79.0       1.8
          89.0       4.0
          90.0       2.2
          91.0      28.0
          92.0       7.2
         102.0       2.0
         103.0       8.9
         104.0      31.9
         105.0      12.7
         106.0       1.1
         115.0      12.9
         116.0       4.0
         117.0      46.2
         118.0      10.0
         120.0       2.2
         128.0       1.9
         129.0       8.7
         130.0     100.0
         131.0      14.3
         132.0       1.3
         145.0       1.6
         146.0       1.4
         174.0      48.6
         175.0       6.6
         176.0       2.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H14 O 0.040 g : 0.5 ml CDCl3
    2-phenylcyclohexanone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.324 B 7.249 C 7.132 D 3.601 E 2.47 F *1 2.25 G *1 2.14 J *1 2.01 K *1 1.82 ASSIGNED BY C-H COSY

         Hz     ppm     Int.
    

       2936.77   7.349    253
       2935.67   7.346    431
       2934.20   7.342    234
       2930.30   7.333    284
       2928.59   7.328   1000
       2927.25   7.325    650
       2922.49   7.313    350
       2921.14   7.310    742
       2920.53   7.308    658
       2919.07   7.305    258
       2904.54   7.268    225
       2903.20   7.265    449
       2901.86   7.262    331
       2895.63   7.246    516
       2893.43   7.240    207
       2888.43   7.228    209
       2855.47   7.145    676
       2854.13   7.142    930
       2852.42   7.138    345
       2848.51   7.128    409
       2847.17   7.125    714
       2846.44   7.123    675
       1447.75   3.623    203
       1442.38   3.610    232
       1435.55   3.593    227
       1430.18   3.579    229
       1004.27   2.513    148
       1002.93   2.510    193
       1000.61   2.504    306
        999.27   2.501    288
        995.97   2.493    247
        994.63   2.489    191
        991.09   2.480    160
        986.33   2.468    151
        985.23   2.466    176
        979.86   2.452    167
        978.64   2.449    172
        974.00   2.438    162
        972.90   2.435    175
        899.90   2.252    143
        897.46   2.246    169
        896.73   2.244    160
        895.63   2.242    165
        894.65   2.239    179
        856.32   2.143    146
        854.00   2.137    201
        852.78   2.134    187
        850.22   2.128    188
        849.00   2.125    173
        848.27   2.123    163
        846.92   2.120    144
        816.89   2.045    157
        813.35   2.036    199
        812.26   2.033    152
        804.93   2.015    172
        803.83   2.012    158
        801.15   2.005    264
        800.29   2.003    273
        799.19   2.000    218
        797.73   1.997    177
        796.39   1.993    164
        795.53   1.991    174
        794.07   1.987    189
        793.33   1.986    194
        791.87   1.982    222
        791.14   1.980    241
        789.55   1.976    237
        788.21   1.973    238
        785.77   1.967    180
        784.55   1.964    163
        735.84   1.842    181
        734.86   1.839    169
        733.03   1.835    238
        731.69   1.831    259
        730.47   1.828    247
        729.00   1.825    218
        728.03   1.822    185
        726.93   1.819    187
        724.12   1.812    301
        722.66   1.809    395
        721.31   1.805    366
        719.97   1.802    321
        715.82   1.792    152
        714.72   1.789    162
        713.87   1.787    151
        712.89   1.784    161
        712.16   1.782    177
        710.94   1.779    182
        709.11   1.775    160
    

in CDCl3



KBr disc



nujol mull



4880 A,200 M,powder