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网站主页CAS数据库列表 4894-75-1更多图谱4-苯基环己酮(4894-75-1)Raman光谱

4-苯基环己酮

产品名称 4-苯基环己酮

CAS号4894-75-1

分子式C12H14O

分子量174.24

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  • Mass

    MS-NW-6827          
    4-phenylcyclohexanone
    C12H14O             (Mass of molecular ion:    174)
    

       Source Temperature: 270 °C
       Sample Temperature: 190 °C
       Reservoir, 75 eV
    

          27.0       7.7
          28.0       3.7
          29.0       4.2
          38.0       1.2
          39.0      11.2
          40.0       1.3
          41.0       7.2
          42.0       1.9
          43.0       1.6
          50.0       4.0
          51.0      10.3
          52.0       3.1
          53.0       2.6
          54.0       1.3
          55.0      12.4
          56.0       4.9
          57.0      20.9
          57.5       2.7
          58.0       8.8
          58.5       1.0
          59.0       2.6
          62.0       1.9
          63.0       6.0
          64.0       2.0
          65.0       7.5
          67.0       1.2
          68.0       1.6
          69.0       1.5
          70.0       1.5
          73.0       3.0
          74.0       1.7
          75.0       1.7
          76.0       2.3
          77.0      11.5
          78.0      12.5
          79.0       2.5
          83.0       2.7
          87.0       1.0
          89.0       4.1
          90.0       1.5
          91.0      71.8
          92.0       6.5
          96.0       1.1
         102.0       3.7
         103.0      12.7
         104.0     100.0
         105.0      12.5
         115.0      21.0
         116.0       6.6
         117.0      62.1
         118.0      23.6
         119.0      66.5
         120.0       7.1
         127.0       2.3
         128.0       3.3
         129.0       5.9
         130.0      14.9
         131.0       5.9
         132.0       4.1
         141.0       2.9
         144.0       1.3
         145.0      16.7
         146.0       6.7
         152.0       1.0
         153.0       1.4
         154.0       2.8
         155.0       1.2
         156.0       2.3
         159.0       3.6
         170.0       1.0
         173.0       1.4
         174.0      92.4
         175.0      12.7
         176.0       1.1
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C12 H14 O 0.042 g : 0.5 ml CDCl3
    4-phenylcyclohexanone
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.319 B 7.24 C 7.23 D 3.019 E 2.51 to 2.490 F *1 2.34 G *1 2.20 J *2 1.96 K *2 1.91

         Hz     ppm     Int.
    

       2935.06   7.345    225
       2934.08   7.342    356
       2932.50   7.338    169
       2929.44   7.331    115
       2927.73   7.326    566
       2926.51   7.323    618
       2925.78   7.321    529
       2921.39   7.310    260
       2919.43   7.305    689
       2917.48   7.301    179
       2899.90   7.257    491
       2898.44   7.253   1000
       2896.24   7.247    589
       2894.29   7.243    197
       2893.43   7.240    244
       2892.82   7.239    262
       2892.33   7.238    294
       2891.60   7.236    500
       2891.11   7.235    555
       2890.26   7.232    604
       2888.79   7.229    287
       2888.06   7.227    431
       2885.86   7.221    127
       2882.32   7.213    124
       2880.86   7.209    192
       2879.52   7.206     95
       1222.41   3.059     63
       1219.12   3.051    117
       1215.58   3.042     68
       1210.33   3.029    128
       1206.91   3.020    235
       1203.49   3.012    124
       1198.24   2.999     70
       1194.82   2.990    125
       1191.41   2.982     63
       1023.07   2.560     66
       1020.63   2.554     34
       1017.46   2.546     63
       1017.09   2.545     62
       1011.23   2.531     86
       1008.67   2.524    325
       1002.56   2.509    623
       1000.37   2.504    382
        999.15   2.501    458
        996.58   2.494    841
        992.07   2.483    913
        988.77   2.475    100
        986.08   2.468     52
        985.11   2.465     58
        899.54   2.251     68
        898.32   2.248     74
        896.24   2.243    140
        895.63   2.242    140
        894.90   2.240    152
        893.55   2.236    172
        892.46   2.234    210
        890.75   2.229    176
        889.04   2.225    180
        888.06   2.223    162
        885.86   2.217    153
        884.77   2.214    150
        882.81   2.209    244
        880.62   2.204    207
        879.64   2.202    279
        877.32   2.196    268
        874.02   2.187    179
        872.19   2.183     62
        870.97   2.180     60
        796.02   1.992    110
        788.94   1.975    100
        788.21   1.973    114
        787.48   1.971    101
        784.06   1.962    187
        782.59   1.959    171
        777.95   1.947    182
        777.10   1.945    189
        776.12   1.942    201
        775.39   1.941    154
        773.93   1.937    114
        771.97   1.932    148
        770.39   1.928    170
        765.63   1.916    160
        764.65   1.914    166
        759.64   1.901     62
        758.91   1.899     65
        757.93   1.897     70
        752.44   1.883     67
    

in CDCl3



KBr disc



nujol mull