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MS-IW-1331 5,6-dimethoxyindole C10H11NO2 (Mass of molecular ion: 177)
Source Temperature: 150 °C Sample Temperature: 120 °C Direct, 75 eV
63.0 2.3 64.0 1.7 76.0 1.3 79.0 1.0 88.5 1.1 89.0 1.8 91.0 4.0 104.0 4.3 105.0 1.0 106.0 6.3 107.0 1.8 116.0 8.4 117.0 1.6 119.0 10.5 132.0 2.3 133.0 2.6 134.0 18.6 135.0 1.7 160.0 1.0 161.0 3.2 162.0 44.0 163.0 4.7 176.0 5.7 177.0 100.0 178.0 11.5 179.0 1.0
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C10 H11 N O2 0.030 g : 0.5 ml DMSO-d6 5,6-dimethoxyindole Assign. Shift(ppm)
A 10.7 B 7.139 C 7.040 D 6.932 E 6.285 F *1 3.762 G *1 3.740
Hz ppm Int.
4294.15 10.745 51 2855.75 7.146 117 2853.18 7.140 156 2850.25 7.132 117 2813.62 7.041 272 2770.39 6.933 236 2514.88 6.293 75 2514.14 6.291 81 2512.86 6.288 95 2512.13 6.286 128 2511.21 6.284 88 2509.93 6.281 82 2509.20 6.279 71 1503.80 3.763 972 1495.00 3.741 1000
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