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MassMS-NW-9483 N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfanilamide C9H10N4O2S2 (Mass of molecular ion: 270)
Source Temperature: 230 °C Sample Temperature: 180 °C Direct, 75 eV
18.0 1.7 27.0 1.4 28.0 1.6 39.0 6.7 41.0 2.7 42.0 1.6 52.0 2.1 53.0 1.3 56.0 3.6 57.0 2.6 58.0 1.4 59.0 9.6 63.0 3.2 64.0 3.7 65.0 38.1 66.0 4.7 74.0 1.4 79.0 1.1 80.0 3.0 90.0 1.0 91.0 3.1 92.0 91.2 93.0 27.3 94.0 1.7 99.0 1.6 103.0 2.3 105.0 1.6 106.0 35.1 107.0 3.6 108.0 65.2 109.0 19.3 110.0 1.4 115.0 1.2 123.0 1.4 124.0 1.6 125.0 2.5 140.0 7.0 147.0 12.9 148.0 1.4 150.0 4.0 156.0 60.3 157.0 5.4 158.0 3.1 162.0 6.3 164.0 2.7 165.0 1.4 205.0 3.1 206.0 24.2 207.0 3.1 208.0 1.2 270.0 100.0 271.0 15.0 272.0 10.1 273.0 1.4
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C9 H10 N4 O2 S2 0.031 g : 0.5 ml DMSO-d6 N-(5-methyl-1,3,4-thiadiazol-2-yl)sulfanilamide 
Assign. Shift(ppm)
A 7.425 B 6.587 C 5.93 E 2.446
Hz ppm Int.2974.73 7.444 36 2972.05 7.437 281 2970.09 7.432 87 2967.90 7.427 23 2967.29 7.425 23 2965.21 7.420 90 2963.26 7.415 284 2960.57 7.408 38 2639.40 6.605 39 2636.72 6.598 290 2634.77 6.593 88 2632.45 6.587 23 2629.88 6.581 87 2628.05 6.576 263 2625.24 6.569 36 977.42 2.446 1000
in DMSO-d6
KBr disc
nujol mull
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