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MS-NW-8032 N-ethyl-4-methoxy-alpha-methylphenethylamine hydrochloride C12H19NO HCl (Mass of molecular ion: 193)
Source Temperature: 190 °C Sample Temperature: 140 °C Direct, 75 eV
18.0 1.7 27.0 1.8 28.0 2.5 29.0 2.3 35.0 1.0 36.0 3.5 38.0 1.1 39.0 1.5 41.0 1.3 42.0 3.3 44.0 18.4 51.0 1.8 52.0 1.5 56.0 2.4 63.0 1.0 65.0 1.6 70.0 1.4 72.0 100.0 73.0 4.8 77.0 4.0 78.0 4.8 79.0 1.1 89.0 1.1 91.0 3.0 121.0 8.0 122.0 1.4 149.0 1.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C12 H19 N O 0.046 g : 0.5 ml CDCl3 N-ethyl-4-methoxy-alpha-methylphenethylamine hydrochloride Assign. Shift(ppm)
A 9.63 B 7.135 C 6.828 D 3.778 E *1 3.504 F 3.33 G 3.11 J *1 2.814 K 1.542 L 1.345 J(E,F)=3.6HZ J(E,J)=-13.0HZ J(F,J)=11.2HZ
Hz ppm Int.
3850.10 9.634 33 2856.45 7.148 163 2854.46 7.143 57 2849.73 7.131 61 2847.75 7.126 186 2733.31 6.840 220 2731.17 6.834 66 2726.59 6.823 61 2724.61 6.818 191 1510.16 3.779 1000 1409.00 3.526 32 1405.49 3.517 36 1396.03 3.494 35 1392.36 3.484 38 1136.63 2.845 45 1125.64 2.817 47 1123.50 2.812 48 1112.52 2.784 40 623.63 1.561 145 616.46 1.543 303 609.13 1.525 137 540.92 1.354 249 534.36 1.338 242
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