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MS-IW-9326 2-bromo-4-fluorotoluene C7H6BrF (Mass of molecular ion: 188)
Source Temperature: 210 °C Sample Temperature: 150 °C Reservoir, 75 eV
31.0 3.0 37.0 1.3 38.0 1.9 39.0 4.8 43.0 1.6 44.0 8.3 50.0 4.5 51.0 3.4 54.0 2.8 56.0 1.3 57.0 10.3 59.0 1.9 61.0 2.5 62.0 4.6 63.0 7.2 68.0 1.0 74.0 1.7 75.0 1.2 80.0 1.7 81.0 6.3 82.0 2.4 83.0 18.5 84.0 3.5 85.0 3.1 86.0 1.3 87.0 1.2 89.0 3.0 94.0 2.5 95.0 2.0 107.0 19.9 108.0 22.6 109.0 100.0 110.0 7.8 187.0 9.4 188.0 48.8 189.0 12.8 190.0 47.2 191.0 3.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H6 Br F 0.05 ml : 0.5 ml CDCl3 2-bromo-4-fluorotoluene Assign. Shift(ppm)
A 7.236 B 7.131 C 6.886 D 2.319
Hz ppm Int.
2897.22 7.250 204 2894.65 7.243 203 2888.92 7.229 202 2886.35 7.223 200 2857.42 7.150 137 2851.32 7.135 149 2848.88 7.129 164 2842.90 7.114 157 2761.47 6.910 122 2758.79 6.904 115 2753.17 6.889 202 2750.61 6.883 190 2744.87 6.869 102 2742.19 6.862 96 926.76 2.319 1000
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