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网站主页CAS数据库列表 14113-05-4更多图谱10-羟基-2-癸烯酸(14113-05-4)质谱(MS)

10-羟基-2-癸烯酸

产品名称 10-羟基-2-癸烯酸

CAS号14113-05-4

分子式C10H18O3

分子量186.25

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  • Mass

    MS-IW-5527          
    trans-10-hydroxy-2-decenoic acid
    C10H18O3            (Mass of molecular ion:    186)
    

       Source Temperature: 160 °C
       Sample Temperature: 150 °C
       Direct, 75 eV
    

          18.0       4.2
          27.0      14.6
          28.0       4.9
          29.0      24.7
          31.0      25.3
          39.0      19.9
          40.0       5.2
          41.0      68.0
          42.0      18.1
          43.0      30.9
          44.0       5.3
          45.0       8.9
          51.0       2.0
          52.0       1.2
          53.0      13.7
          54.0      35.9
          55.0     100.0
          56.0      11.0
          57.0      18.4
          58.0       4.6
          59.0       2.3
          60.0       3.3
          61.0       1.1
          65.0       2.8
          66.0       5.9
          67.0      61.6
          68.0      50.6
          69.0      18.0
          70.0      13.6
          71.0      24.2
          72.0       6.3
          73.0      35.3
          74.0       2.0
          77.0       2.7
          78.0       2.4
          79.0      16.6
          80.0      21.3
          81.0      67.4
          82.0      29.6
          83.0      20.7
          84.0      18.3
          85.0      13.2
          86.0      58.7
          87.0       8.2
          88.0       1.0
          91.0       2.7
          93.0      14.1
          94.0      13.8
          95.0      30.4
          96.0      30.4
          97.0      29.4
          98.0      20.1
          99.0      39.4
         100.0      23.4
         101.0       5.6
         102.0       1.3
         104.0       1.0
         106.0       3.8
         107.0       6.6
         108.0      31.0
         109.0      15.3
         110.0       3.2
         111.0       8.6
         112.0       6.2
         113.0       6.9
         114.0       4.0
         115.0       1.2
         117.0       1.7
         119.0       1.0
         120.0       1.0
         121.0       6.8
         122.0      10.6
         123.0       8.2
         124.0      27.8
         125.0       8.5
         126.0       5.0
         127.0       3.4
         132.0       1.5
         135.0       2.2
         137.0       1.4
         138.0       8.4
         139.0       6.4
         140.0       7.4
         141.0       1.1
         150.0       7.4
         151.0       1.5
         156.0      10.5
         157.0       1.1
         168.0      19.2
         169.0       7.6
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H18 O3 0.031 g : 0.5 ml CDCl3
    trans-10-hydroxy-2-decenoic acid
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.061 B 7.0 C 5.820 D 3.643 E 2.224 F 1.57 G 1.47 J 1.36 to 1.32 J(A,C)=15.6HZ J(C,E)=-1.6HZ

         Hz     ppm     Int.
    

       2837.16   7.100    112
       2830.20   7.082    242
       2823.12   7.064    126
       2821.53   7.061    127
       2814.58   7.043    262
       2807.50   7.025    131
       2335.08   5.843    150
       2333.50   5.839    339
       2331.91   5.835    156
       2319.46   5.804    150
       2317.87   5.800    318
       2316.28   5.796    137
       1463.01   3.661    466
       1456.30   3.644   1000
       1449.71   3.628    503
        900.51   2.254     95
        899.05   2.250    102
        893.43   2.236    243
        892.09   2.233    269
        885.74   2.217    262
        878.91   2.200    114
        877.32   2.196    110
        639.77   1.601     36
        633.18   1.585    125
        625.98   1.567    198
        619.02   1.549    169
        612.30   1.533     65
        601.81   1.506     38
        594.73   1.489    116
        587.89   1.472    176
        583.25   1.460    113
        580.93   1.454    138
        573.85   1.436     56
        553.96   1.387     40
        547.49   1.370    114
        546.02   1.367    114
        531.37   1.330    919
    

in CDCl3



KBr disc



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