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联苯-4-甲酰氯

产品名称 联苯-4-甲酰氯

CAS号14002-51-8

分子式C13H9ClO

分子量216.66

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  • Mass

    MS-IW-0590          
    4-biphenylcarbonyl chloride
    C13H9ClO            (Mass of molecular ion:    216)
    

       Source Temperature: 140 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          51.0       1.4
          63.0       2.7
          75.0       1.8
          75.5       2.2
          76.0      11.3
          76.5       3.8
          77.0       1.9
          90.5       4.4
          94.0       1.1
         102.0       1.0
         126.0       1.6
         127.0       2.2
         150.0       2.0
         151.0       7.6
         152.0      29.8
         153.0      28.7
         154.0       3.7
         181.0     100.0
         182.0      14.5
         183.0       1.2
         216.0      26.0
         217.0       3.8
         218.0       8.7
         219.0       1.2
    

90 MHz in CDCl3

400 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C13 H9 Cl O 0.045 g : 0.5 ml CDCl3
    4-biphenylcarbonyl chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.158 B 7.70 C 7.62 D 7.49 E 7.42 C,D AND E WERE CONFIRMED BY LAOCN PROGRAM. 400MHZ : HSP-41-772

         Hz     ppm     Int.
    

        737.75   8.238     89
        735.81   8.216    735
        735.25   8.210    413
        733.81   8.194    243
        729.06   8.141    268
        727.00   8.118    994
        725.13   8.097    160
        695.56   7.767    154
        693.69   7.746   1000
        691.63   7.723    302
        689.94   7.704    115
        688.56   7.689    189
        686.94   7.671    341
        685.44   7.654    561
        684.88   7.648    781
        683.94   7.637    339
        681.19   7.606    327
        680.06   7.594    553
        678.44   7.576    619
        675.19   7.539    280
        673.88   7.525    303
        673.06   7.516    233
        671.44   7.498    562
        670.75   7.490    538
        669.38   7.475    438
        668.38   7.463    284
        667.06   7.449    358
        665.94   7.436    506
        663.69   7.411    540
    


  • 1H NMR 399.65 MHz
    C13 H9 Cl O saturated in CDCl3
    4-biphenylcarbonyl chloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.196 B 7.711 C 7.648 D 7.485 E 7.420 90MHZ : HSP-02-728

         Hz     ppm     Int.
    

       3285.03   8.220     31
       3283.81   8.217     46
       3281.86   8.212    155
       3280.03   8.208    819
       3278.08   8.203    368
       3275.63   8.197     71
       3275.02   8.195     69
       3273.32   8.191    295
       3271.36   8.186   1000
       3269.65   8.182    225
       3267.58   8.177     47
       3266.72   8.174     33
       3091.43   7.736     31
       3090.94   7.735     37
       3089.84   7.732     45
       3087.65   7.726    161
       3085.82   7.722    861
       3083.86   7.717    336
       3081.42   7.711     71
       3081.05   7.710     69
       3079.22   7.705    281
       3077.15   7.700    854
       3075.44   7.696    181
       3073.61   7.691     61
       3072.88   7.689     50
       3072.39   7.688     45
       3072.02   7.687     47
       3071.41   7.686     43
       3070.56   7.684     43
       3069.95   7.682     41
       3069.70   7.681     41
       3068.85   7.679     45
       3067.87   7.677     45
       3067.02   7.675     51
       3066.04   7.672     52
       3064.94   7.670     64
       3062.13   7.663    428
       3060.67   7.659    641
       3058.72   7.654    212
       3055.05   7.645    288
       3054.69   7.644    290
       3053.71   7.641    615
       3053.22   7.640    555
       3052.49   7.638    590
       3050.42   7.633    113
       3048.71   7.629     37
       3005.37   7.521     30
       3004.03   7.517     31
       3003.30   7.515     39
       3002.69   7.514     43
       3000.61   7.509    206
       2999.51   7.506    342
       2997.80   7.502    154
       2996.34   7.498     78
       2992.43   7.488    699
       2990.97   7.484    388
       2988.16   7.477     68
       2986.21   7.473    213
       2984.74   7.469    426
       2984.25   7.468    376
       2981.32   7.460     77
       2980.10   7.457     45
       2979.74   7.456     41
       2979.13   7.455     37
       2978.39   7.453     31
       2977.66   7.451     34
       2976.81   7.449     37
       2976.32   7.448     32
       2975.95   7.447     34
       2975.22   7.445     37
       2974.37   7.443     44
       2972.05   7.437    184
       2970.70   7.434    326
       2969.36   7.430    200
       2967.04   7.425     42
       2966.67   7.424     40
       2965.70   7.421    121
       2963.38   7.415    356
       2961.06   7.410     93
       2959.72   7.406     34
       2957.40   7.400     72
       2956.18   7.397    119
       2954.83   7.394     71
       2954.10   7.392     37
    

in CDCl3



KBr disc



nujol mull