parameter in CS2+TMS
-
1H NMR 300 MHz C8 H9 N 10 wt% in CS2+TMS(2 : 1vol) 2-methyl-5-vinylpyridine Parameter ppm Hz
D(A) 8.380 D(B) 7.437 D(C) 6.914 D(D) 6.569 D(E) 5.170 D(F) 5.643 D(G) 2.430 J(A,B) 2.37 J(A,C) 0.86 J(A,D) -0.52 J(A,E) 0.12 J(A,F) 0.1 J(A,G) 0.2 J(B,C) 7.99 J(B,D) -0.53 J(B,E) 0.12 J(B,F) 0.0 J(B,G) 0.3 J(C,D) 0.50 J(C,E) 0.0 J(C,F) 0.0 J(C,G) -0.48 J(D,E) 10.96 J(D,F) 17.62 J(D,G) 0.25 J(E,F) 0.96 J(E,G) -0.25 J(F,G) -0.25 ROWBOTHAM,J.B. & SCHAEFER,T. CAN.J.CHEM. 52, 136 (1974)
Hz ppm Int.
2515.19 8.384 137 2512.87 8.376 139 2236.44 7.455 83 2234.06 7.447 82 2228.36 7.428 90 2226.10 7.420 89 2078.12 6.927 128 2070.10 6.900 113 1985.39 6.618 65 1974.44 6.581 69 1967.75 6.559 74 1956.80 6.523 78 1701.87 5.673 131 1701.04 5.670 132 1684.23 5.614 114 1683.46 5.612 114 1556.83 5.189 126 1556.05 5.187 125 1545.88 5.153 120 1545.10 5.150 118 729.02 2.430 1000
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