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MS-NW-1752 p-(1,1,3,3-tetramethylbutyl)phenol C14H22O (Mass of molecular ion: 206)
Source Temperature: 150 °C Sample Temperature: 120 °C Direct, 75 eV
18.0 1.1 27.0 2.1 29.0 4.8 39.0 3.8 41.0 11.6 43.0 2.3 51.0 1.2 53.0 1.0 55.0 2.1 57.0 10.5 65.0 2.2 77.0 3.6 79.0 1.1 91.0 4.1 95.0 3.8 107.0 10.6 119.0 2.5 121.0 1.5 134.0 2.9 135.0 100.0 136.0 10.3 206.0 4.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C14 H22 O 0.048 g : 0.5 ml CDCl3 p-(1,1,3,3-tetramethylbutyl)phenol Assign. Shift(ppm)
A 7.21 B 6.75 C 5.00 D 1.687 E 1.329 F 0.715
Hz ppm Int.
650.88 7.268 63 648.63 7.243 23 644.31 7.195 24 642.00 7.169 92 607.94 6.789 109 605.56 6.762 26 601.31 6.715 22 599.00 6.689 70 447.31 4.995 91 151.13 1.688 185 119.00 1.329 596 66.44 0.742 34 66.31 0.741 34 65.88 0.736 35 64.00 0.715 1000
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