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MS-NW-8328 tris(2-chloroethyl) phosphite C6H12Cl3O3P (Mass of molecular ion: 268)
Source Temperature: 260 °C Sample Temperature: 130 °C Reservoir, 75 eV
15.0 2.1 26.0 2.5 27.0 44.6 28.0 14.2 29.0 2.4 31.0 13.0 36.0 2.1 43.0 3.2 44.0 1.6 45.0 5.0 47.0 8.0 49.0 3.7 51.0 1.3 62.0 12.6 63.0 100.0 64.0 6.2 65.0 42.6 77.0 3.2 81.0 1.7 82.0 2.4 83.0 14.7 91.0 8.3 109.0 11.8 110.0 2.0 117.0 4.7 119.0 1.6 127.0 13.5 129.0 4.6 135.0 2.2 143.0 2.3 145.0 18.7 147.0 6.5 171.0 18.8 173.0 6.2 189.0 32.5 190.0 1.5 191.0 20.8 193.0 3.5 207.0 17.0 209.0 10.9 211.0 1.8 233.0 29.9 234.0 2.1 235.0 19.3 236.0 1.3 237.0 3.2
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H12 Cl3 O3 P 0.05 ml : 0.5 ml CDCl3 tris(2-chloroethyl) phosphite Assign. Shift(ppm)
A 4.108 B 3.677
Hz ppm Int.
1655.52 4.143 38 1651.61 4.133 480 1649.05 4.127 81 1646.12 4.119 694 1645.26 4.117 459 1643.92 4.114 508 1640.14 4.104 561 1638.43 4.100 661 1637.57 4.098 442 1635.01 4.092 72 1632.32 4.085 505 1479.86 3.703 47 1475.22 3.692 816 1469.24 3.677 1000 1463.50 3.662 695
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