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MS-IW-8149 5-bromo-1,2,3-trifluorobenzene C6H2BrF3 (Mass of molecular ion: 210)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
31.0 4.6 37.0 1.7 50.0 1.2 56.0 1.7 57.0 1.5 61.0 5.3 62.0 5.3 68.0 3.0 74.0 1.4 75.0 2.5 79.0 1.9 80.0 6.0 81.0 44.1 82.0 2.5 92.0 1.8 93.0 1.2 99.0 3.2 105.0 3.9 106.0 3.9 111.0 1.7 112.0 3.8 130.0 4.8 131.0 70.3 132.0 4.7 210.0 100.0 211.0 6.8 212.0 97.7 213.0 6.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C6 H2 Br F3 0.05 ml : 0.5 ml CDCl3 5-bromo-1,2,3-trifluorobenzene Assign. Shift(ppm)
A 7.159
Hz ppm Int.
2875.85 7.196 68 2874.27 7.192 30 2872.44 7.188 121 2869.75 7.181 137 2867.80 7.176 684 2861.57 7.161 898 2860.96 7.159 1000 2854.86 7.144 686 2850.22 7.132 139 2846.68 7.123 78
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