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MS-NW-4763 N,N-dimethyl-p-nitrosoaniline C8H10N2O (Mass of molecular ion: 150)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 4.6 17.0 1.1 18.0 5.5 27.0 2.0 28.0 2.0 29.0 1.7 30.0 3.3 37.0 1.6 38.0 2.9 39.0 6.6 40.0 1.2 41.0 2.4 42.0 36.0 43.0 2.3 44.0 4.2 50.0 8.4 51.0 8.4 52.0 4.7 53.0 2.3 54.0 1.1 61.0 1.0 62.0 2.0 63.0 8.6 64.0 3.9 65.0 7.0 66.0 4.0 67.0 1.3 68.0 2.6 69.0 1.7 74.0 3.1 75.0 2.9 76.0 6.5 77.0 35.7 78.0 15.8 79.0 20.2 80.0 3.8 81.0 1.4 90.0 6.4 91.0 17.2 92.0 10.7 93.0 5.8 94.0 2.4 102.0 1.0 103.0 3.5 104.0 22.3 105.0 37.1 106.0 3.8 107.0 1.0 117.0 2.3 118.0 13.7 119.0 26.4 120.0 37.4 121.0 5.2 132.0 1.6 133.0 2.5 134.0 2.1 135.0 2.1 136.0 3.7 147.0 2.1 148.0 2.7 150.0 100.0 151.0 10.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H10 N2 O 0.029 g : 0.5 ml CDCl3 N,N-dimethyl-p-nitrosoaniline Assign. Shift(ppm)
A 7.79 B 6.654 C 3.138 90MHZ : HSP-06-120 AT ROOM TEMP
Hz ppm Int.
702.69 7.847 27 702.31 7.842 27 701.63 7.835 26 694.13 7.751 30 693.50 7.744 31 600.19 6.702 83 599.00 6.689 42 592.13 6.612 39 590.75 6.597 68 281.06 3.139 1000