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MassMS-NW-3703 1,10-undecadiene C11H20 (Mass of molecular ion: 152)
Source Temperature: 260 °C Sample Temperature: 180 °C Reservoir, 75 eV
26.0 1.0 27.0 18.8 28.0 2.4 29.0 25.4 39.0 27.3 40.0 4.1 41.0 100.0 42.0 10.2 43.0 15.0 51.0 1.6 53.0 10.1 54.0 73.5 55.0 99.5 56.0 11.2 57.0 8.0 65.0 1.7 66.0 4.3 67.0 69.5 68.0 44.1 69.0 60.6 70.0 6.1 77.0 1.1 79.0 2.5 80.0 2.3 81.0 50.0 82.0 55.3 83.0 12.3 84.0 1.3 94.0 1.0 95.0 28.3 96.0 23.4 97.0 4.5 109.0 11.3 110.0 8.1 111.0 1.9 123.0 3.0 124.0 5.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C11 H20 0.04 ml : 0.5 ml CDCl3 1,10-undecadiene 
Assign. Shift(ppm)
A 5.79 B 4.98 C 4.92 D 2.04 E 1.29
Hz ppm Int.541.06 6.042 51 534.56 5.969 105 531.13 5.931 60 528.06 5.897 57 524.63 5.858 133 524.00 5.851 93 518.19 5.786 84 517.38 5.777 171 513.94 5.739 96 510.81 5.704 92 507.50 5.667 203 501.00 5.595 114 456.88 5.102 76 455.38 5.085 162 454.44 5.075 173 453.94 5.069 125 453.06 5.059 306 451.56 5.042 153 447.50 4.997 137 446.31 4.984 275 445.13 4.971 204 443.94 4.957 148 442.81 4.945 75 439.63 4.909 49 438.19 4.893 108 437.63 4.887 156 437.25 4.883 155 436.38 4.873 308 435.88 4.867 289 435.19 4.860 212 434.44 4.851 175 432.81 4.833 46 192.19 2.146 45 191.50 2.139 46 190.38 2.126 50 185.75 2.075 151 179.31 2.003 170 173.13 1.934 69 135.25 1.511 36 130.44 1.457 106 125.88 1.406 90 115.88 1.294 1000 111.06 1.241 68 101.25 1.131 34
in CDCl3
liquid film
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