400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C17 H14 N4 S 0.040 g : 0.5 ml CDCl3 1,5-diphenyl-3-(2-thienyl)formazan Assign. Shift(ppm)
A 14.23 B 7.63 C 7.62 D 7.42 E 7.25 F 7.25 G 7.068 J(B,F)=1.2HZ. J(B,G)=3.8HZ. J(F,G)=5.1HZ. 90MHZ. : HSP-03-424
Hz ppm Int.
5685.30 14.226 276 3066.89 7.674 36 3065.92 7.672 42 3063.23 7.665 46 3062.01 7.662 53 3060.79 7.659 50 3054.69 7.644 376 3053.47 7.641 413 3050.78 7.634 861 3049.56 7.631 1000 3047.61 7.626 278 3041.99 7.612 877 3041.02 7.610 804 3039.06 7.605 138 2984.62 7.469 31 2983.15 7.465 34 2977.78 7.451 78 2975.83 7.447 165 2974.12 7.442 577 2972.17 7.437 233 2966.80 7.424 850 2960.21 7.408 247 2958.50 7.403 568 2956.54 7.398 100 2908.69 7.279 55 2907.96 7.277 57 2905.27 7.270 227 2904.05 7.267 352 2903.08 7.265 231 2898.19 7.252 515 2896.97 7.249 767 2893.07 7.240 369 2891.85 7.236 351 2890.63 7.233 179 2889.40 7.230 243 2888.43 7.228 140 2828.61 7.078 328 2824.95 7.069 331 2823.49 7.065 308 2819.82 7.056 281
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1H NMR 89.56 MHz C17 H14 N4 S 0.040 g : 0.5 ml CDCl3 1,5-diphenyl-3-(2-thienyl)formazan Assign. Shift(ppm)
A 14.19 B 7.64 C 7.61 D 7.42 E 7.25 F 7.24 G 7.069 400MHZ. : HSP-41-319
Hz ppm Int.
1271.29 14.195 293 688.38 7.687 413 686.52 7.666 737 681.54 7.610 807 679.69 7.590 1000 678.61 7.578 994 676.17 7.550 254 673.24 7.518 404 671.58 7.499 471 669.34 7.474 285 665.04 7.426 952 657.03 7.337 628 654.00 7.303 562 652.25 7.283 505 650.88 7.268 385 647.07 7.225 759 646.09 7.215 690 643.75 7.188 150 641.80 7.167 128 641.31 7.161 125 640.82 7.156 139 640.43 7.151 139 636.62 7.109 355 633.01 7.069 314 631.45 7.051 213 627.83 7.011 171
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