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MS-IW-7236 1-(chloro(1-pyrrolidinyl)methylene)pyrrolidinium hexafluorophosphate C9H16ClF6N2P (Mass of molecular ion: 332)
Source Temperature: 180 °C Sample Temperature: 230 °C Direct, 75 eV
15.0 2.4 17.0 2.8 18.0 14.1 20.0 5.7 26.0 1.7 27.0 8.1 28.0 18.6 29.0 5.5 30.0 8.1 35.0 1.9 36.0 20.4 37.0 1.6 38.0 7.2 39.0 13.9 40.0 8.3 41.0 35.5 42.0 17.7 43.0 13.2 44.0 15.0 49.0 2.5 50.0 1.5 51.0 1.1 53.0 3.0 54.0 3.9 55.0 73.5 56.0 35.5 57.0 1.7 58.0 9.2 60.0 1.0 62.0 2.8 64.0 1.3 66.0 1.8 67.0 16.0 68.0 10.6 69.0 19.4 70.0 100.0 71.0 11.1 72.0 1.4 76.0 3.7 78.0 2.0 81.0 1.0 82.0 1.9 83.0 1.7 84.0 1.0 85.0 43.3 88.0 6.0 89.0 1.2 90.0 1.3 91.0 1.7 95.0 1.1 96.0 2.2 97.0 3.2 98.0 63.2 99.0 10.0 104.0 49.8 107.0 20.7 112.0 1.0 113.0 1.1 117.0 1.2 120.0 1.7 125.0 8.0 126.0 1.0 129.0 3.2 139.0 1.1 140.0 5.4 141.0 1.3 145.0 2.9 151.0 1.1 153.0 1.1 158.0 2.3 160.0 1.0 164.0 3.0 168.0 34.3 169.0 4.1 171.0 1.3 187.0 3.6 189.0 1.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C9 H16 Cl F6 N2 P 0.040 g : 0.5 ml CDCl3 1-(chloro(1-pyrrolidinyl)methylene)pyrrolidinium hexafluorophosphate Assign. Shift(ppm)
A 3.892 B 2.077
Hz ppm Int.
1562.03 3.909 338 1555.62 3.893 833 1549.21 3.877 367 836.79 2.094 372 832.94 2.085 493 830.16 2.078 1000 827.60 2.071 507 823.54 2.061 385
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