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MassMS-NW-1721 N-phenyl-2-naphthylamine C16H13N (Mass of molecular ion: 219)
Source Temperature: 190 °C Sample Temperature: 120 °C Direct, 75 eV
39.0 2.2 50.0 1.2 51.0 4.0 63.0 2.2 65.0 1.8 75.0 1.6 77.0 3.9 89.0 1.8 94.5 1.7 95.5 3.0 96.5 1.5 101.0 1.5 102.0 2.8 107.5 1.3 108.5 11.4 109.0 4.0 109.5 5.9 110.0 1.0 114.0 1.0 115.0 10.1 116.0 3.5 126.0 2.2 127.0 3.4 128.0 1.0 140.0 1.2 153.0 1.1 165.0 1.3 178.0 1.0 189.0 2.5 190.0 1.5 191.0 3.4 192.0 2.8 204.0 1.2 216.0 4.6 217.0 21.7 218.0 34.3 219.0 100.0 220.0 17.5 221.0 1.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C16 H13 N 0.034 g : 0.5 ml CDCl3 N-phenyl-2-naphthylamine 
Assign. Shift(ppm)
A 7.72 B 7.71 C 7.618 D 7.40 E 7.39 F 7.29 G 7.28 J 7.181 K 7.131 L 6.964 M 5.80 ASSIGNED BY H-H AND C-H COSY.
Hz ppm Int.3089.23 7.730 393 3088.62 7.729 406 3086.55 7.724 561 3081.18 7.710 438 3080.44 7.708 445 3077.64 7.701 588 3049.44 7.631 369 3048.71 7.629 369 3041.26 7.610 435 3040.53 7.608 432 2958.74 7.404 785 2957.15 7.400 677 2951.78 7.386 379 2950.44 7.383 518 2949.10 7.380 259 2946.66 7.374 58 2943.60 7.366 311 2942.26 7.363 296 2923.10 7.315 113 2921.02 7.309 569 2918.70 7.304 504 2917.36 7.300 451 2915.89 7.297 189 2913.70 7.291 838 2912.48 7.288 982 2910.52 7.283 735 2909.30 7.280 452 2907.10 7.275 323 2905.15 7.270 818 2903.69 7.266 357 2902.47 7.263 315 2875.49 7.196 504 2873.17 7.190 502 2866.70 7.174 467 2864.38 7.168 451 2860.35 7.158 48 2859.99 7.157 48 2859.50 7.156 48 2856.08 7.147 181 2854.25 7.142 801 2853.15 7.140 1000 2851.07 7.134 303 2847.53 7.126 274 2846.56 7.123 442 2845.70 7.121 749 2844.60 7.118 659 2842.29 7.112 121 2791.50 6.985 211 2790.41 6.983 382 2789.31 6.980 216 2787.60 6.976 45 2786.74 6.973 49 2784.42 6.968 285 2784.06 6.967 294 2783.08 6.964 641 2782.10 6.962 295 2776.86 6.949 193 2775.76 6.946 320 2774.66 6.943 169 2316.04 5.796 273
in CDCl3
CCl4 solution
KBr disc
nujol mull
OXIDATION WITH O2 IN TOLUENE/ALKALINE ALCOHOL
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