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网站主页CAS数据库列表 134-91-8更多图谱二(4-二乙氨基苯基)甲醇(134-91-8)红外图谱(IR2)

二(4-二乙氨基苯基)甲醇

产品名称 二(4-二乙氨基苯基)甲醇

CAS号134-91-8

分子式C21H30N2O

分子量326.48

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  • Mass

    MS-IW-7567          
    4,4'-bis(diethylamino)benzhydryl alcohol
    C21H30N2O           (Mass of molecular ion:    326)
    

       Source Temperature: 170 °C
       Sample Temperature: 170 °C
       Direct, 75 eV
    

          17.0       1.0
          18.0       5.0
          28.0       1.2
          29.0       1.9
          77.0       2.2
          78.0       1.1
          79.0       1.0
          90.0       1.0
          91.0       2.0
          96.5       1.0
         104.0       2.1
         105.0       1.8
         106.0       3.1
         111.0       1.3
         112.0       5.8
         112.5       1.0
         117.0       1.2
         118.0      10.2
         119.0       5.6
         120.0       5.7
         125.0       1.6
         126.0       5.8
         126.5       1.1
         127.0       1.8
         132.0       7.7
         133.0       5.1
         134.0       9.1
         140.0      16.5
         140.5       3.7
         141.0       2.1
         146.0       2.0
         147.0       6.7
         147.5       3.6
         148.0      18.9
         148.5       3.7
         149.0       2.3
         150.0      15.2
         151.0       2.0
         152.0       1.0
         155.0       4.1
         155.5       3.1
         160.0       1.4
         162.0       4.9
         163.0       4.7
         165.0       3.7
         166.0       1.7
         176.0      12.9
         177.0       2.1
         178.0       4.1
         194.0       1.6
         221.0       2.2
         222.0       1.0
         223.0       4.8
         224.0       1.1
         235.0       1.2
         237.0       3.9
         238.0       2.3
         239.0       2.2
         251.0      16.7
         252.0       4.0
         253.0       1.3
         265.0      12.5
         266.0       4.0
         267.0      13.4
         268.0       2.7
         279.0       2.5
         280.0       1.5
         281.0       5.7
         282.0       3.8
         283.0       1.1
         293.0       2.2
         295.0     100.0
         296.0      23.4
         297.0       2.9
         307.0       1.2
         309.0      80.2
         310.0      68.8
         311.0      56.6
         312.0      11.4
         313.0       1.3
         323.0       1.1
         324.0      12.5
         325.0      10.3
         326.0      46.2
         327.0      10.7
         328.0       1.3
         335.0       1.6
         350.0       1.5
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C21 H30 N2 O 0.040 g : 0.5 ml CDCl3
    4,4'-bis(diethylamino)benzhydryl alcohol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.20 B 6.628 C 5.662 D 3.317 E 2.01 F 1.129

         Hz     ppm     Int.
    

       2880.98   7.209    214
       2879.27   7.205     97
       2874.15   7.192     73
       2872.44   7.188    234
       2872.07   7.187    221
       2653.44   6.640    239
       2651.37   6.635     79
       2646.61   6.623     74
       2644.53   6.618    234
       2642.33   6.612     50
       2264.65   5.667     44
       2261.35   5.659     46
       1336.67   3.345    121
       1329.59   3.327    403
       1322.63   3.310    431
       1315.55   3.292    162
        806.76   2.019     53
        803.22   2.010     54
        458.13   1.147    466
        455.81   1.141     94
        451.17   1.129   1000
        448.73   1.123    206
        444.09   1.112    494
        441.65   1.106     95
    

in CDCl3



KBr disc



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