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MassMS-NW-8544 chloro(p-chlorophenyl)phenylmethane C13H10Cl2 (Mass of molecular ion: 236)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
18.0 1.6 36.0 5.0 38.0 2.0 39.0 5.8 50.0 4.1 51.0 6.2 52.0 1.0 62.0 3.5 63.0 8.7 64.0 1.1 65.0 2.4 69.0 1.7 69.5 6.7 70.0 1.5 73.0 1.8 74.0 3.0 75.0 4.9 76.0 2.1 77.0 3.6 81.0 3.6 81.5 7.5 82.0 20.5 82.5 18.2 83.0 12.5 83.5 1.6 86.0 2.0 87.0 3.1 88.0 1.4 89.0 5.4 91.0 1.2 99.0 2.1 100.0 2.1 100.5 1.3 101.0 1.9 105.0 3.5 111.0 1.8 113.0 2.9 114.0 1.6 115.0 4.4 125.0 1.9 126.0 1.5 127.0 1.3 137.0 1.2 138.0 1.4 139.0 8.3 140.0 1.1 151.0 1.2 152.0 2.7 162.0 1.5 163.0 10.5 164.0 11.9 165.0 100.0 166.0 74.0 167.0 20.0 168.0 2.2 199.0 3.9 200.0 1.1 201.0 97.7 202.0 17.7 203.0 31.9 204.0 5.6 216.0 1.2 236.0 1.1
90 MHz in CDCl3
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1H NMR 89.56 MHz C13 H10 Cl2 0.05 ml : 0.5 ml CDCl3 chloro(p-chlorophenyl)phenylmethane 
Assign. Shift(ppm)
A 7.34 to 7.31 B 7.28 C 6.047
Hz ppm Int.665.00 7.426 26 662.19 7.394 49 661.56 7.387 49 656.00 7.325 327 654.75 7.311 386 652.00 7.281 1000 650.06 7.259 119 646.94 7.224 52 645.13 7.204 30 643.75 7.188 23 642.88 7.179 24 541.69 6.049 190
in CDCl3
liquid film
4880 A,200 M,liquid
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