-
MassMS-IW-7559 N-fluorobenzenesulfonimide C12H10FNO4S2 (Mass of molecular ion: 315)
Source Temperature: 180 °C Sample Temperature: 140 °C Direct, 75 eV
39.0 1.8 50.0 3.6 51.0 17.2 52.0 1.1 63.0 1.0 64.0 1.7 65.0 2.6 75.0 1.0 76.0 1.4 77.0 89.0 78.0 6.5 91.0 1.6 97.0 2.2 125.0 7.6 140.0 1.9 141.0 100.0 142.0 7.8 143.0 5.2 233.0 1.0 315.0 5.5
400 MHz in CDCl3
-
1H NMR 399.65 MHz C12 H10 F N O4 S2 0.039 g : 0.5 ml CDCl3 N-fluorobenzenesulfonimide 
Assign. Shift(ppm)
A 8.012 B 7.769 C 7.604
Hz ppm Int.3206.54 8.024 770 3205.57 8.021 836 3198.12 8.003 980 3196.90 8.000 806 3114.50 7.794 166 3113.28 7.791 268 3112.06 7.787 178 3107.30 7.776 245 3105.71 7.772 581 3104.13 7.768 243 3099.37 7.756 256 3098.14 7.753 389 3096.92 7.750 222 3047.85 7.627 227 3046.26 7.623 742 3044.56 7.619 352 3038.70 7.604 922 3037.96 7.602 1000 3032.23 7.588 279 3030.52 7.583 527 3028.93 7.579 168
in CDCl3
KBr disc
nujol mull
更多供应商
