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MassMS-NW-9945 4-(trimethylsilyl)morpholine C7H17NOSi (Mass of molecular ion: 159)
Source Temperature: 210 °C Sample Temperature: 160 °C Reservoir, 75 eV
15.0 1.5 27.0 3.4 28.0 15.7 29.0 19.4 30.0 8.4 31.0 4.1 41.0 2.6 42.0 7.4 43.0 11.3 44.0 4.8 45.0 22.3 46.0 1.5 47.0 2.2 52.0 1.2 54.0 1.8 55.0 6.6 56.0 13.4 57.0 28.9 57.5 2.1 58.0 6.3 59.0 52.4 60.0 4.1 61.0 3.3 66.0 2.9 70.0 3.7 71.0 2.1 72.0 4.1 73.0 81.0 74.0 7.3 75.0 22.8 76.0 1.7 77.0 2.4 85.0 1.7 86.0 100.0 87.0 32.3 88.0 5.3 89.0 2.4 93.0 1.2 100.0 16.8 101.0 83.4 102.0 10.2 103.0 9.8 114.0 13.5 115.0 2.3 116.0 1.6 128.0 1.6 129.0 11.0 130.0 2.0 131.0 2.2 144.0 74.5 145.0 9.2 146.0 3.5 147.0 34.7 148.0 5.5 149.0 3.3 158.0 20.2 159.0 71.6 160.0 11.2 161.0 3.3 229.0 1.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H17 N O Si 0.05 ml : 0.5 ml CDCl3 4-(trimethylsilyl)morpholine 
Assign. Shift(ppm)
A 3.550 B 2.827 C 0.044
Hz ppm Int.1423.71 3.563 139 1419.19 3.552 154 1414.43 3.540 163 1134.64 2.840 150 1129.88 2.828 158 1125.24 2.816 159 22.22 0.056 47 21.24 0.054 76 17.82 0.045 1000 14.77 0.037 144
in CDCl3
liquid film
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