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雙(3,5-二甲-4-羥苯)碸

产品名称 雙(3,5-二甲-4-羥苯)碸

CAS号13288-70-5

分子式C16H18O4S

分子量306.38

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  • Mass

    MS-IW-4872          
    4,4'-sulfonylbis(2,6-xylenol)
    C16H18O4S           (Mass of molecular ion:    306)
    

       Source Temperature: 170 °C
       Sample Temperature: 170 °C
       Direct, 75 eV
    

          18.0       2.0
          27.0       1.7
          39.0       4.3
          41.0       3.5
          43.0       3.4
          51.0       3.1
          52.0       1.5
          53.0       5.7
          55.0       1.7
          63.0       1.9
          65.0       6.4
          66.0       1.0
          67.0       1.9
          69.0       1.3
          77.0      15.6
          78.0       3.0
          79.0       3.5
          81.0       2.2
          89.0       1.3
          91.0      17.3
          92.0       2.6
          93.0       2.6
          95.0       1.1
         103.0       1.5
         107.0       4.0
         108.0       2.1
         109.0       2.3
         119.0       1.7
         120.0       2.0
         121.0      18.3
         121.5       1.6
         122.0      32.2
         123.0       5.5
         137.0      17.5
         138.0      98.7
         139.0       9.0
         141.0       1.6
         153.0       1.8
         154.0       1.1
         169.0      57.6
         170.0      39.5
         171.0       6.4
         172.0       2.2
         183.0       1.0
         185.0       1.2
         211.0       1.9
         212.0       1.7
         225.0       1.1
         226.0       2.2
         227.0       2.3
         241.0       2.5
         242.0       6.5
         243.0       1.3
         305.0       1.4
         306.0     100.0
         307.0      19.3
         308.0       7.1
         309.0       1.0
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C16 H18 O4 S 0.040 g : 0.5 ml DMSO-d6
    4,4'-sulfonylbis(2,6-xylenol)
    ChemicalStructure
        Assign.     Shift(ppm)
    A 9.32 B 7.493 C 2.210

         Hz     ppm     Int.
    

       3723.60   9.318    148
       2994.84   7.494    376
        883.33   2.211   1000
    

in DMSO-d6



KBr disc



nujol mull