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MassMS-IW-9043 3-methyl-1-hexanol C7H16O (Mass of molecular ion: 116)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.0 18.0 3.8 27.0 19.3 28.0 4.5 29.0 20.7 31.0 19.2 39.0 15.8 40.0 2.8 41.0 64.8 42.0 22.8 43.0 94.0 44.0 4.6 45.0 5.6 46.0 2.2 51.0 1.3 53.0 4.7 54.0 3.0 55.0 96.0 56.0 46.2 57.0 14.4 59.0 1.3 67.0 3.2 68.0 3.6 69.0 81.6 70.0 100.0 71.0 16.7 72.0 1.3 73.0 1.1 81.0 1.0 83.0 13.8 84.0 1.3 85.0 2.0 97.0 1.1 98.0 14.5 99.0 1.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H16 O 0.05 ml : 0.5 ml CDCl3 3-methyl-1-hexanol 
Assign. Shift(ppm)
A 3.644 B 2.74 C 1.58 D *1 1.37 to 1.35 E *1 1.13 F 0.886 G 0.884
Hz ppm Int.1101.20 2.756 96 1096.31 2.744 216 1091.31 2.731 91 653.44 1.636 42 648.19 1.622 65 646.73 1.619 56 645.75 1.616 51 641.24 1.605 97 640.50 1.603 103 638.92 1.599 59 635.38 1.590 101 633.54 1.586 108 630.37 1.578 116 629.27 1.575 110 628.54 1.573 109 626.59 1.568 100 624.51 1.563 115 619.75 1.551 93 614.38 1.538 49 613.40 1.535 53 612.30 1.533 46 553.83 1.386 119 548.58 1.373 119 547.97 1.372 125 546.39 1.368 149 544.43 1.363 93 542.60 1.358 111 541.14 1.355 153 540.53 1.353 152 539.18 1.350 116 535.28 1.340 112 531.98 1.332 102 529.91 1.326 154 524.66 1.313 165 523.19 1.310 160 519.41 1.300 110 517.94 1.296 136 515.87 1.291 137 514.53 1.288 109 513.55 1.285 101 512.21 1.282 143 511.60 1.281 141 508.67 1.273 128 505.62 1.266 104 500.49 1.253 95 457.40 1.145 90 454.35 1.137 73 452.03 1.132 72 449.83 1.126 88 446.78 1.118 66 444.46 1.113 70 361.21 0.904 476 356.45 0.892 1000 354.13 0.887 928 349.61 0.875 910 346.80 0.868 523
in CDCl3
liquid film
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