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MassMS-IW-4909 phenyl 1-hydroxy-2-naphthoate C17H12O3 (Mass of molecular ion: 264)
Source Temperature: 150 °C Sample Temperature: 110 °C Direct, 75 eV
39.0 2.9 51.0 1.3 63.0 2.6 65.0 3.2 66.0 1.3 88.0 1.7 89.0 2.7 94.0 5.6 113.0 2.6 114.0 10.7 115.0 20.4 116.0 1.9 142.0 1.9 143.0 9.3 144.0 1.0 170.0 29.8 171.0 100.0 172.0 12.1 173.0 1.0 264.0 28.4 265.0 5.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C17 H12 O3 0.048 g : 0.5 ml CDCl3 phenyl 1-hydroxy-2-naphthoate 
Assign. Shift(ppm)
A 11.74 B 8.426 C 7.959 D 7.771 E 7.617 F 7.527 G 7.448 J 7.33 K 7.30 L 7.242
Hz ppm Int.4692.91 11.743 1000 3372.83 8.440 157 3372.10 8.438 177 3371.55 8.437 181 3364.40 8.419 173 3363.85 8.417 186 3363.12 8.416 194 3185.45 7.971 414 3176.66 7.949 445 3110.90 7.785 168 3110.35 7.783 160 3102.66 7.764 220 3052.47 7.638 122 3051.19 7.635 134 3045.51 7.621 175 3044.23 7.618 248 3042.95 7.615 121 3037.45 7.601 148 3036.17 7.598 138 3016.20 7.548 141 3014.92 7.544 154 3009.24 7.530 108 3007.78 7.527 215 3006.49 7.523 155 3000.82 7.509 101 2999.72 7.506 103 2988.00 7.477 36 2985.80 7.472 195 2983.78 7.466 99 2980.67 7.459 54 2979.57 7.456 116 2978.29 7.453 370 2977.55 7.451 362 2975.36 7.445 91 2973.34 7.440 39 2971.88 7.437 133 2970.04 7.432 331 2967.66 7.426 68 2933.59 7.341 269 2927.18 7.325 99 2926.08 7.322 236 2924.99 7.319 362 2920.22 7.307 92 2918.57 7.303 251 2916.93 7.299 102 2912.35 7.288 72 2911.25 7.285 117 2909.97 7.282 74 2901.17 7.260 75 2900.81 7.259 81 2899.34 7.255 374 2898.24 7.252 478 2896.05 7.247 142 2894.03 7.242 45 2892.75 7.239 122 2891.83 7.236 209 2890.73 7.234 367 2889.63 7.231 346 2887.07 7.224 63
in CDCl3
KBr disc
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