图谱信息 供应商 相关产品
网站主页CAS数据库列表 13138-53-9更多图谱4-硝基邻苯二甲酰胺(13138-53-9)Raman光谱

4-硝基邻苯二甲酰胺

产品名称 4-硝基邻苯二甲酰胺

CAS号13138-53-9

分子式C8H7N3O4

分子量209.16


  • Mass

    MS-KW-0591          
    4-nitrophthalamide 
    C8H7N3O4            (Mass of molecular ion:    209)
    

       Source Temperature: 170 °C
       Sample Temperature: 170 °C
       Direct, 75 eV
    

          16.0       5.7
          17.0       8.8
          18.0       4.4
          28.0       3.1
          30.0      12.9
          37.0       2.6
          38.0       2.3
          44.0       3.6
          50.0       3.1
          51.0       2.5
          52.0       1.7
          53.0       1.6
          61.0       1.8
          62.0       3.8
          63.0       5.0
          64.0       1.4
          65.0       1.3
          70.0       1.0
          73.0       3.4
          74.0      19.9
          75.0      63.3
          76.0       5.9
          77.0       1.1
          89.0       1.4
          90.0       2.1
          91.0       3.1
         100.0       1.4
         101.0       1.6
         102.0      11.8
         103.0      87.6
         104.0       7.6
         106.0       2.4
         117.0       1.5
         118.0       1.3
         119.0       3.9
         127.0       1.1
         129.0       1.3
         145.0       3.8
         146.0      13.0
         147.0      11.4
         148.0       9.7
         149.0      21.4
         150.0       5.1
         162.0       7.8
         163.0       1.2
         175.0       1.4
         176.0       2.2
         191.0      18.6
         192.0     100.0
         193.0      39.8
         194.0       4.2
         209.0       2.2
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C8H7N3O4 0.040 g : 0.5 ml DMSO-d6
    4-nitrophthalamide
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.315 B 8.285 C *1 8.06 D *1 8.00 E 7.706 F *1 7.62

         Hz     ppm     Int.
    

       3329.47   8.329    415
       3327.15   8.323    493
       3321.17   8.308    416
       3318.97   8.302    604
       3312.99   8.287   1000
       3310.92   8.282    679
       3220.95   8.057    434
       3196.66   7.996    443
       3084.72   7.716    746
       3076.42   7.696    701
       3045.78   7.619    844
    

in DMSO-d6



KBr disk



Nujol