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MS-IW-2178 1-(m-tolyl)piperazine dihydrochloride C11H16N2 2HCl (Mass of molecular ion: 176)
Source Temperature: 150 °C Sample Temperature: 140 °C Direct, 75 eV
17.0 1.8 18.0 8.2 27.0 2.0 28.0 5.8 29.0 4.9 30.0 3.6 35.0 3.4 36.0 21.1 37.0 1.2 38.0 6.8 39.0 3.5 41.0 2.3 42.0 3.2 51.0 2.1 52.0 1.0 56.0 9.8 57.0 5.0 63.0 2.3 65.0 6.8 77.0 2.5 78.0 1.1 88.0 1.2 89.0 2.1 90.0 1.4 91.0 15.0 92.0 2.2 105.0 3.7 117.0 1.1 118.0 9.1 119.0 13.8 120.0 6.7 121.0 1.7 132.0 1.1 134.0 100.0 135.0 10.3 146.0 1.3 175.0 1.3 176.0 29.6 177.0 3.8
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C11 H16 N2 0.035 g : 0.5 ml DMSO-d6 1-(m-tolyl)piperazine dihydrochloride Assign. Shift(ppm)
A 9.83 B 7.245 C 7.05 D 7.021 E 6.878 F 6.10 G 3.546 J 3.321 K 2.298
Hz ppm Int.
3929.60 9.833 90 2903.90 7.267 94 2895.97 7.247 187 2888.18 7.227 124 2819.21 7.055 175 2810.21 7.032 111 2802.12 7.012 88 2752.69 6.888 129 2745.21 6.870 117 2438.81 6.103 221 1422.42 3.560 239 1417.69 3.548 340 1412.35 3.534 284 1327.51 3.322 264 918.73 2.299 1000
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