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MassMS2014-05016CW benz(cd)indol-2(1H)-one C11H7NO (Mass of molecular ion: 169)
Source Temperature: 250 °C Sample Temperature: 25 °C Direct, 70 eV
18.0 2.5 38.0 1.0 39.0 2.3 50.0 2.1 51.0 1.8 56.5 1.8 57.0 6.1 57.5 2.7 61.0 1.6 62.0 4.9 63.0 8.3 64.0 2.3 69.5 1.3 70.0 2.9 70.5 14.7 71.0 3.8 74.0 3.6 75.0 3.2 76.0 1.8 84.5 10.7 85.0 2.5 86.0 3.9 87.0 6.0 88.0 9.3 89.0 1.9 98.0 1.0 99.0 1.1 111.0 1.0 112.0 1.4 113.0 21.9 114.0 44.9 115.0 6.4 126.0 1.6 139.0 2.0 140.0 59.0 141.0 51.6 142.0 6.2 168.0 3.8 169.0 100.0 170.0 34.6 171.0 2.5 203.0 3.6 205.0 1.2
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C11 H7 N O 0.025 g : 0.5 ml DMSO-d6 benz(cd)indol-2(1H)-one 
Assign. Shift(ppm)
A 10.83 B 8.187 C 8.051 D 7.825 E 7.617 F 7.526 G 7.027 J(B,D)=8.1HZ J(C,D)=7.0HZ J(E,F)=8.2HZ J(F,G)=7.0HZ
Hz ppm Int.4330.29 10.836 317 3276.52 8.199 728 3272.40 8.189 30 3268.43 8.179 827 3221.59 8.062 726 3217.77 8.052 37 3214.57 8.044 854 3134.61 7.844 650 3131.87 7.837 41 3130.95 7.835 39 3127.59 7.826 610 3126.53 7.824 620 3123.93 7.817 40 3119.51 7.806 510 3049.32 7.630 631 3040.92 7.609 1000 3014.83 7.544 640 3007.81 7.527 691 3006.29 7.523 430 2999.42 7.506 452 2997.28 7.500 36 2811.89 7.036 848 2808.38 7.028 37 2805.02 7.019 806
in DMSO-d6
KBr disc
nujol mull
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