双(3-氯苄)胺

Mass

MS-IW-8355          
bis(3-chlorobenzyl)amine
C14H13Cl2N          (Mass of molecular ion:    265)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      39.0       2.1
      50.0       1.8
      51.0       2.6
      63.0       4.2
      65.0       1.9
      73.0       1.3
      75.0       3.2
      76.0       1.1
      77.0       5.4
      89.0      14.0
      90.0       6.0
      91.0      41.9
      92.0       3.4
      99.0       5.1
     101.0       1.8
     102.0       1.5
     106.0       1.7
     111.0       1.8
     112.0       1.3
     113.0       3.0
     115.0       1.0
     117.0       1.3
     125.0     100.0
     126.0      30.4
     127.0      34.2
     128.0       9.9
     137.0       3.9
     138.0       3.1
     139.0       2.7
     140.0      99.9
     141.0       8.8
     142.0      31.9
     143.0       2.7
     152.0       6.0
     153.0       1.0
     154.0      17.2
     155.0       1.7
     156.0       4.9
     230.0       3.3
     232.0       1.0
     262.0       1.7
     263.0       2.4
     264.0       9.3
     265.0       8.2
     266.0       6.6
     267.0       4.6
     268.0       1.6

Assign. Shift(ppm) A 7.325 B 7.22 to 7.19 C 3.730 D 1.61

     Hz     ppm     Int.

   2929.57   7.331    299
   2927.73   7.326    468
   2897.09   7.250     69
   2889.77   7.231    264
   2889.28   7.230    241
   2885.13   7.220    348
   2883.42   7.215    711
   2882.57   7.213   1000
   2880.62   7.208    483
   2877.08   7.200    165
   2875.37   7.195    355
   2873.90   7.192    306
   2873.29   7.190    272
   2871.83   7.186    183
   2869.14   7.180    111
   2868.29   7.178     95
   2867.19   7.175    135
   2866.70   7.174    138
   2865.11   7.170     95
   1490.97   3.731    988
    642.70   1.609    133