图谱信息 供应商 相关产品
网站主页CAS数据库列表 1287-13-4更多图谱二茂钌(1287-13-4)核磁图(13CNMR)

二茂钌

产品名称 二茂钌

CAS号1287-13-4

分子式C10H10Ru10*

分子量231.26

展开


  • Mass

    MS-NW-9958          
    bis(eta-cyclopentadienyl)ruthenium(II)
    C10H10Ru            (Mass of molecular ion:    232)
    

       Source Temperature: 130 °C
       Sample Temperature: 100 °C
       Direct, 75 eV
    

          18.0       1.0
         101.0       1.2
         102.0       2.3
         104.0       1.4
         111.0       1.1
         112.0       1.3
         113.0       2.0
         114.0       3.2
         114.5       2.2
         115.0       2.7
         115.5       3.1
         116.0       6.4
         117.0       3.4
         137.0       1.5
         138.0       2.6
         139.0       3.7
         140.0       2.8
         141.0       3.9
         143.0       1.5
         150.0       1.0
         151.0       1.4
         152.0       1.4
         153.0       1.4
         161.0       3.0
         163.0       1.5
         164.0       7.0
         165.0       7.3
         166.0       9.5
         167.0      16.9
         168.0       1.0
         169.0       9.7
         175.0       1.2
         176.0       1.5
         177.0       2.1
         178.0       2.4
         179.0       1.3
         180.0       1.5
         200.0       1.1
         201.0       2.2
         202.0       3.1
         203.0       4.5
         204.0       5.7
         205.0       3.3
         206.0       4.6
         207.0       1.0
         208.0       1.3
         226.0      17.1
         227.0       3.0
         228.0       7.8
         229.0      39.3
         230.0      43.3
         231.0      56.3
         232.0     100.0
         233.0      10.9
         234.0      56.4
         235.0       6.2
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C10 H10 Ru 0.040 g : 0.5 ml CDCl3
    bis(eta-cyclopentadienyl)ruthenium(II)
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.552

         Hz     ppm     Int.
    

       1823.49   4.563     37
       1819.58   4.553   1000
       1814.94   4.542     41
    

in CDCl3



KBr disc



nujol mull