图谱信息 供应商 相关产品
网站主页CAS数据库列表 1270-98-0更多图谱三氯一茂钛(1270-98-0)核磁图(13CNMR)

三氯一茂钛

产品名称 三氯一茂钛

CAS号1270-98-0

分子式C5H5Cl3Ti5*

分子量219.32

展开


  • Mass

    MS-NW-9914          
    trichloro(eta-cyclopentadienyl)titanium(IV)
    C5H5Cl3Ti           (Mass of molecular ion:    218)
    

       Source Temperature: 150 °C
       Sample Temperature: 120 °C
       Direct, 75 eV
    

          36.0       1.4
          38.0       1.5
          39.0      10.0
          48.0       1.0
          63.0       2.7
          65.0     100.0
          66.0       5.8
          83.0       7.0
          84.0       1.0
          85.0       3.9
          86.0       1.2
         118.0       7.3
         119.0       1.1
         120.0       5.5
         121.0       2.1
         122.0       3.3
         146.0       1.1
         147.0       1.9
         148.0       7.0
         149.0       1.5
         150.0       2.7
         181.0       2.2
         182.0       4.9
         183.0      18.3
         184.0       5.4
         185.0      12.3
         186.0       2.1
         187.0       2.6
         216.0       2.7
         217.0       2.7
         218.0      27.0
         219.0       5.8
         220.0      26.4
         221.0       4.0
         222.0       9.5
         223.0       1.2
         224.0       1.4
    

400 MHz in CDCl3


  • 1H NMR 399.65 MHz
    C5 H5 Cl3 Ti 0.031 g : 0.5 ml CDCl3
    trichloro(eta-cyclopentadienyl)titanium(IV)
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.047 B 6.907

         Hz     ppm     Int.
    

       2820.80   7.059     32
       2816.41   7.048   1000
       2811.65   7.036     27
       2760.50   6.908    481
    

in CDCl3



KBr disc



nujol mull