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MassMS-NW-9078 bis(triphenyltin) oxide C36H30OSn2 (Mass of molecular ion: 718)
Source Temperature: 220 °C Sample Temperature: 170 °C Direct, 75 eV
17.0 1.2 18.0 7.1 28.0 1.0 39.0 1.0 50.0 1.8 51.0 5.4 52.0 1.7 76.0 1.0 77.0 6.6 78.0 12.5 112.0 1.2 116.0 16.6 117.0 9.1 118.0 27.9 119.0 10.3 120.0 37.5 122.0 5.4 124.0 6.5 135.0 1.3 137.0 1.9 145.0 1.2 152.0 3.3 153.0 2.7 154.0 8.0 155.0 1.0 189.0 1.1 193.0 16.4 194.0 10.2 195.0 27.8 196.0 11.9 197.0 36.7 198.0 2.6 199.0 5.3 201.0 6.4 266.0 1.1 268.0 1.2 269.0 2.4 270.0 17.2 271.0 13.2 272.0 28.6 273.0 16.6 274.0 35.8 275.0 5.3 276.0 5.4 277.0 1.4 278.0 6.5 279.0 1.9 280.0 2.2 280.5 1.1 281.0 2.4 282.0 2.0 286.0 1.5 287.0 3.8 288.0 3.9 289.0 6.1 290.0 4.7 291.0 6.0 292.0 1.1 293.0 1.2 295.0 1.0 331.0 1.0 343.0 3.0 345.0 3.1 346.0 2.6 347.0 43.9 348.0 31.8 349.0 77.0 350.0 40.1 351.0 100.0 352.0 19.3 353.0 15.7 354.0 3.1 355.0 16.8 356.0 3.3 406.0 1.0 408.0 1.0 423.0 1.8 424.0 1.5 425.0 3.3 426.0 1.9 427.0 4.2 428.0 1.1 479.0 1.1 480.0 1.3 481.0 3.1 482.0 3.2 483.0 6.0 484.0 4.6 485.0 6.5 486.0 3.7 487.0 5.2 488.0 1.7 489.0 2.0 491.0 1.4 557.0 1.4 558.0 1.5 559.0 3.0 560.0 2.5 561.0 3.4 562.0 2.2 563.0 2.7 564.0 1.2 565.0 1.2 621.0 1.3 622.0 1.0 623.0 1.5 625.0 1.2 633.0 3.3 635.0 8.6 637.0 18.1 638.0 14.2 639.0 20.5 640.0 12.0 641.0 16.3 642.0 2.4 643.0 6.8 645.0 4.2 714.0 1.8 716.0 1.9 718.0 1.5
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C36 H30 O Sn2 0.038 g : 0.5 ml DMSO-d6 bis(triphenyltin) oxide 
Assign. Shift(ppm)
A 7.48 B 7.33 C 7.30
Hz ppm Int.3076.54 7.699 112 3018.80 7.554 110 3011.96 7.537 104 2991.21 7.485 911 2984.86 7.469 993 2964.23 7.418 295 2943.60 7.366 188 2942.14 7.362 178 2939.09 7.355 271 2936.40 7.348 557 2929.44 7.331 652 2927.61 7.326 503 2924.07 7.317 999 2916.87 7.299 1000 2910.16 7.282 390
in DMSO-d6
KBr disc
nujol mull
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