壬二酰氯

Mass

MS-NW-9895          
azelaoyl dichloride
C9H14Cl2O2          (Mass of molecular ion:    224)

   Source Temperature: 260 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      18.0       2.1
      26.0       1.1
      27.0      15.5
      28.0       5.8
      29.0      10.7
      35.0       1.8
      36.0      18.0
      38.0       5.9
      39.0      12.6
      40.0       2.8
      41.0      37.1
      42.0      12.6
      43.0      11.1
      44.0       1.6
      51.0       1.2
      53.0       4.7
      54.0       6.9
      55.0     100.0
      56.0       7.9
      57.0       3.7
      63.0       4.8
      65.0       1.8
      67.0      16.7
      68.0      10.5
      69.0      17.5
      70.0       4.2
      77.0       2.6
      78.0       7.0
      79.0       6.2
      80.0      11.2
      81.0      11.4
      82.0       7.9
      83.0      26.1
      84.0      29.0
      85.0       2.0
      91.0       2.6
      92.0       1.1
      93.0       4.7
      95.0       4.0
      96.0       5.9
      97.0      13.3
      98.0      18.3
      99.0       1.2
     105.0       1.0
     107.0       4.8
     108.0       1.0
     109.0       4.9
     110.0       2.3
     111.0       8.8
     117.0       1.0
     124.0      13.6
     125.0       9.5
     135.0       2.7
     152.0       1.6
     153.0      13.6
     154.0       1.3
     189.0       8.1
     191.0       2.7

Assign. Shift(ppm) A 2.89 B 1.71 C 1.39 D 1.35

     Hz     ppm     Int.

    271.25   3.029     35
    266.56   2.977    400
    259.44   2.897   1000
    252.38   2.818    639
    170.06   1.899     34
    167.31   1.869     66
    159.50   1.781    189
    157.94   1.764    171
    153.00   1.709    271
    149.13   1.666    187
    147.19   1.644    215
    146.50   1.636    216
    141.56   1.581    123
    141.25   1.578    121
    140.63   1.571    123
    139.06   1.553    112
    138.81   1.550    112
    136.63   1.526     87
    136.06   1.520     86
    135.94   1.518     86
    135.06   1.509     90
    134.00   1.497     97
    128.31   1.433    252
    121.00   1.352    757