图谱信息 供应商 相关产品
网站主页CAS数据库列表 123-98-8更多图谱壬二酰氯(123-98-8)核磁图(13CNMR)

壬二酰氯

产品名称 壬二酰氯

CAS号123-98-8

分子式C9H14Cl2O2

分子量225.11

展开


  • Mass

    MS-NW-9895          
    azelaoyl dichloride
    C9H14Cl2O2          (Mass of molecular ion:    224)
    

       Source Temperature: 260 °C
       Sample Temperature: 150 °C
       Reservoir, 75 eV
    

          18.0       2.1
          26.0       1.1
          27.0      15.5
          28.0       5.8
          29.0      10.7
          35.0       1.8
          36.0      18.0
          38.0       5.9
          39.0      12.6
          40.0       2.8
          41.0      37.1
          42.0      12.6
          43.0      11.1
          44.0       1.6
          51.0       1.2
          53.0       4.7
          54.0       6.9
          55.0     100.0
          56.0       7.9
          57.0       3.7
          63.0       4.8
          65.0       1.8
          67.0      16.7
          68.0      10.5
          69.0      17.5
          70.0       4.2
          77.0       2.6
          78.0       7.0
          79.0       6.2
          80.0      11.2
          81.0      11.4
          82.0       7.9
          83.0      26.1
          84.0      29.0
          85.0       2.0
          91.0       2.6
          92.0       1.1
          93.0       4.7
          95.0       4.0
          96.0       5.9
          97.0      13.3
          98.0      18.3
          99.0       1.2
         105.0       1.0
         107.0       4.8
         108.0       1.0
         109.0       4.9
         110.0       2.3
         111.0       8.8
         117.0       1.0
         124.0      13.6
         125.0       9.5
         135.0       2.7
         152.0       1.6
         153.0      13.6
         154.0       1.3
         189.0       8.1
         191.0       2.7
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C9 H14 Cl2 O2 0.05 ml : 0.5 ml CDCl3
    azelaoyl dichloride
    ChemicalStructure
        Assign.     Shift(ppm)
    A 2.89 B 1.71 C 1.39 D 1.35

         Hz     ppm     Int.
    

        271.25   3.029     35
        266.56   2.977    400
        259.44   2.897   1000
        252.38   2.818    639
        170.06   1.899     34
        167.31   1.869     66
        159.50   1.781    189
        157.94   1.764    171
        153.00   1.709    271
        149.13   1.666    187
        147.19   1.644    215
        146.50   1.636    216
        141.56   1.581    123
        141.25   1.578    121
        140.63   1.571    123
        139.06   1.553    112
        138.81   1.550    112
        136.63   1.526     87
        136.06   1.520     86
        135.94   1.518     86
        135.06   1.509     90
        134.00   1.497     97
        128.31   1.433    252
        121.00   1.352    757
    

in CDCl3



liquid film