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MassMS-IW-2607 1,2-epoxy-3-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyloxy)propane C11H9F13O2 (Mass of molecular ion: 420)
Source Temperature: 200 °C Sample Temperature: 160 °C Reservoir, 75 eV
15.0 5.0 19.0 2.6 26.0 1.5 27.0 16.3 28.0 10.0 29.0 54.0 30.0 10.8 31.0 100.0 32.0 1.8 33.0 2.4 39.0 2.7 40.0 2.5 41.0 2.5 42.0 3.0 43.0 25.1 44.0 56.4 45.0 20.9 47.0 3.9 49.0 2.3 51.0 11.2 55.0 3.2 56.0 2.4 57.0 75.5 58.0 75.6 59.0 5.4 63.0 2.4 64.0 2.0 65.0 7.1 69.0 26.0 71.0 3.2 73.0 2.1 75.0 1.8 77.0 11.8 78.0 2.3 87.0 2.7 89.0 1.1 93.0 1.0 95.0 5.2 100.0 2.8 108.0 1.2 109.0 1.8 113.0 1.1 115.0 1.1 119.0 5.0 131.0 5.3 169.0 1.5 327.0 4.0 377.0 2.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C11 H9 F13 O2 0.05 ml : 0.5 ml CDCl3 1,2-epoxy-3-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyloxy)propane 
Assign. Shift(ppm)
A *1 3.84 B 3.80 C *1 3.395 D 3.155 E 2.804 F 2.620 G 2.434
Hz ppm Int.1545.90 3.869 135 1542.72 3.861 31 1539.06 3.852 279 1536.01 3.844 327 1532.35 3.835 692 1529.42 3.827 1000 1522.58 3.810 482 1520.75 3.806 670 1518.07 3.799 689 1516.48 3.795 678 1513.55 3.788 165 1509.77 3.778 325 1506.71 3.771 268 1499.88 3.753 132 1365.60 3.417 555 1359.74 3.403 612 1354.13 3.389 481 1348.14 3.374 550 1268.19 3.174 186 1265.63 3.167 359 1264.04 3.163 250 1262.82 3.160 298 1262.33 3.159 288 1261.47 3.157 411 1259.64 3.152 365 1258.67 3.150 308 1256.96 3.146 211 1255.49 3.142 333 1252.81 3.135 163 1125.49 2.817 664 1121.34 2.806 726 1120.48 2.804 835 1116.33 2.794 702 1050.90 2.630 638 1048.22 2.623 631 1045.90 2.618 570 1043.21 2.611 539 998.54 2.499 106 991.70 2.482 198 984.86 2.465 108 983.52 2.461 89 979.74 2.452 205 973.02 2.435 371 966.19 2.418 190 962.65 2.409 97 961.06 2.405 125 954.35 2.388 215 947.51 2.371 106
liquid film
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