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MassMS-NW-3497 2-phenoxypropionyl chloride C9H9ClO2 (Mass of molecular ion: 184)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
26.0 2.8 27.0 8.0 28.0 3.5 29.0 1.0 36.0 2.8 37.0 1.4 38.0 3.9 39.0 14.3 40.0 2.2 43.0 4.5 50.0 6.0 51.0 17.0 52.0 1.2 55.0 3.2 56.0 1.7 60.5 1.5 62.0 1.8 63.0 6.7 64.0 2.0 65.0 14.6 66.0 8.7 74.0 1.5 75.0 1.3 76.0 2.0 77.0 59.7 78.0 5.6 91.0 18.0 92.0 2.9 93.0 11.2 94.0 24.6 95.0 1.9 103.0 2.5 119.0 2.5 120.0 14.1 121.0 100.0 122.0 9.0 184.0 14.0 185.0 1.5 186.0 5.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C9 H9 Cl O2 0.04 ml : 0.5 ml CDCl3 2-phenoxypropionyl chloride 
Assign. Shift(ppm)
A 7.27 B 7.01 C 6.87 D 4.916 E 1.708
Hz ppm Int.661.63 7.388 51 660.94 7.380 33 660.31 7.373 84 658.44 7.352 48 655.06 7.315 42 653.50 7.297 182 652.31 7.284 66 651.56 7.276 143 650.31 7.262 44 647.19 7.227 89 645.56 7.209 193 644.81 7.200 180 642.50 7.174 45 635.25 7.094 56 633.81 7.077 125 632.63 7.064 105 628.94 7.023 41 626.69 6.998 149 624.13 6.969 40 620.69 6.931 87 619.19 6.914 221 617.75 6.898 297 615.44 6.872 62 612.13 6.835 71 610.50 6.817 140 609.31 6.804 151 450.75 5.033 58 443.94 4.957 186 437.13 4.881 196 430.38 4.806 68 156.38 1.747 1000 149.63 1.671 953
in CDCl3
liquid film
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