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网站主页CAS数据库列表 120-29-6更多图谱托品醇(120-29-6)质谱(MS)

托品醇

产品名称 托品醇

CAS号120-29-6

分子式C8H15NO

分子量141.21

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  • Mass

    MS-NW-4801          
    tropine
    C8H15NO             (Mass of molecular ion:    141)
    

       Source Temperature: 260 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          15.0       6.7
          17.0       5.1
          18.0      24.4
          26.0       1.2
          27.0       8.4
          28.0       5.2
          29.0       4.3
          30.0       4.3
          31.0       1.2
          39.0       8.2
          40.0       1.5
          41.0      11.9
          42.0      49.1
          43.0       5.3
          44.0       9.2
          51.0       1.4
          52.0       1.0
          53.0       3.1
          54.0       5.3
          55.0      17.8
          56.0      10.8
          57.0      26.3
          58.0       4.5
          65.0       1.3
          66.0       1.1
          67.0      14.6
          68.0      11.0
          69.0       3.3
          70.0      11.3
          71.0       1.4
          77.0       1.1
          80.0       2.4
          81.0       4.6
          82.0     100.0
          83.0      78.6
          84.0       9.6
          86.0       1.4
          93.0       1.1
          94.0       8.2
          95.0       2.6
          96.0      81.2
          97.0      32.6
          98.0       3.8
         112.0      13.7
         113.0      23.8
         114.0       1.7
         122.0       1.4
         124.0      43.0
         125.0       4.0
         126.0       1.9
         140.0       1.5
         141.0      33.8
         142.0       3.2
    

90 MHz in CDCl3

400 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C8 H15 N O 0.043 g : 0.5 ml CDCl3
    tropine
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 1.65 B *1 1.93 to 2.23 C 2.252 D 2.59 E 3.070 F 4.012

         Hz     ppm     Int.
    

        201.69   2.253   1000
        183.56   2.050    245
        181.06   2.022    232
        178.13   1.989     95
        177.75   1.985     97
        177.06   1.977     97
        154.25   1.723     84
    


  • 1H NMR 399.65 MHz
    C8 H15 N O 0.037 g : 0.5 ml CDCl3
    tropine
    ChemicalStructure
        Assign.     Shift(ppm)
    A 4.000 B 3.062 C 2.77 D 2.246 E 2.09 F 2.08 G 1.98 J 1.658

         Hz     ppm     Int.
    

       1597.53   3.998     55
       1592.41   3.985     30
       1227.42   3.072     73
       1223.51   3.062     90
       1220.83   3.055     79
       1108.52   2.774    118
        897.58   2.246   1000
        848.02   2.122     37
        843.26   2.110     61
        842.41   2.108     62
        839.36   2.101     51
        834.84   2.089    121
        829.47   2.076    103
        827.76   2.072    155
        826.90   2.070    154
        824.95   2.065     79
        822.14   2.058     63
        795.65   1.991     75
        790.65   1.979     65
        787.60   1.971     48
        786.50   1.968     56
        783.20   1.960     39
        669.56   1.676     99
        668.70   1.674    105
        655.64   1.641     87
        654.66   1.639     87
        653.93   1.637     83
    

in CDCl3



KBr disc



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