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网站主页CAS数据库列表 120-00-3更多图谱固蓝 BB(120-00-3)核磁图(13CNMR)

固蓝 BB

产品名称 固蓝 BB

CAS号120-00-3

分子式C17H20N2O3

分子量300.35

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  • Mass

    MS-NW-7805          
    Fast Blue BB base
    C17H20N2O3          (Mass of molecular ion:    300)
    

       Source Temperature: 180 °C
       Sample Temperature: 180 °C
       Direct, 75 eV
    

          18.0       1.3
          26.0       1.0
          27.0       5.8
          28.0       2.3
          29.0       7.1
          39.0       2.4
          40.0       1.2
          41.0       4.6
          42.0       5.8
          43.0       1.4
          50.0       2.9
          51.0      10.2
          52.0       2.5
          53.0       1.2
          54.0       2.2
          65.0       1.4
          66.0       2.5
          67.0       3.0
          68.0       6.7
          69.0       1.2
          70.0       3.0
          76.0       2.5
          77.0      43.0
          78.0       3.8
          82.0       1.1
          83.0       1.1
          93.0       1.3
          94.0       4.7
          95.0       1.5
          96.0       1.4
         105.0     100.0
         106.0       8.0
         109.0       1.2
         110.0       1.6
         111.0      11.7
         112.0       1.0
         122.0       1.7
         123.0       4.9
         124.0       1.5
         137.0       1.8
         139.0       6.7
         140.0       1.1
         151.0       1.5
         152.0       1.3
         153.0       1.8
         165.0       1.6
         167.0       3.9
         168.0       2.1
         195.0       5.2
         197.0       1.0
         225.0       1.8
         243.0       1.2
         271.0      22.9
         272.0       4.8
         300.0      43.6
         301.0       9.3
         302.0       1.2
    

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C17 H20 N2 O3 0.033 g : 0.5 ml CDCl3
    fast blue bb base
    ChemicalStructure
        Assign.     Shift(ppm)
    A 8.44 B 8.174 C 7.866 D 7.52 E 7.46 F 6.374 G *1 4.106 J *1 4.027 K 3.76 L 1.42 CONFIRMED BY LAOCN PROGRAM

         Hz     ppm     Int.
    

        755.50   8.436     81
        732.13   8.175    308
        709.63   7.924    140
        707.31   7.898    146
        704.13   7.863    147
        703.25   7.853    139
        702.19   7.841    102
        700.81   7.826    125
        699.75   7.814    171
        677.81   7.569     78
        677.13   7.561     83
        676.06   7.549    107
        673.81   7.524    391
        671.63   7.500    279
        668.75   7.468    151
        668.25   7.462    149
        666.88   7.447    147
        570.94   6.375    346
        378.38   4.225     91
        375.69   4.195     42
        374.94   4.187     45
        371.31   4.146    336
        369.00   4.121     58
        364.31   4.068    515
        361.38   4.036     54
        357.25   3.989    348
        350.38   3.913     98
        337.06   3.764    143
        133.63   1.493    525
        131.31   1.467     93
        130.44   1.457     99
        126.63   1.414   1000
        119.69   1.337    451
    

in CDCl3



KBr disc



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