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MS-IW-0732 2-amino-4-tert-butylphenol C10H15NO (Mass of molecular ion: 165)
Source Temperature: 120 °C Sample Temperature: 110 °C Direct, 75 eV
28.0 1.0 39.0 1.6 41.0 1.9 51.0 1.4 53.0 1.8 55.0 1.2 61.0 2.0 65.0 2.1 75.0 1.7 77.0 3.3 79.0 2.9 80.0 1.7 89.0 1.0 91.0 2.1 92.0 2.1 93.0 1.8 103.0 1.7 105.0 9.7 106.0 2.7 107.0 1.2 109.0 7.0 110.0 5.7 117.0 1.2 121.0 1.0 122.0 9.0 123.0 1.3 133.0 26.6 134.0 5.7 135.0 2.5 149.0 2.3 150.0 100.0 151.0 10.5 164.0 1.3 165.0 56.8 166.0 6.6
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C10 H15 N O 0.035 g : 0.5 ml DMSO-d6 2-amino-4-tert-butylphenol Assign. Shift(ppm)
A 8.7 B 6.639 C 6.545 D 6.399 E 4.4 F 1.189
Hz ppm Int.
2654.42 6.642 86 2652.13 6.637 88 2620.39 6.557 75 2612.30 6.537 97 2562.10 6.411 53 2559.66 6.405 50 2553.86 6.391 41 2551.57 6.385 40 475.31 1.190 1000
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