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MS-NW-7683 1-bromo-2,4-dichlorobenzene C6H3BrCl2 (Mass of molecular ion: 224)
Source Temperature: 270 °C Sample Temperature: 170 °C Reservoir, 75 eV
36.0 1.6 37.0 5.3 38.0 2.5 49.0 3.6 50.0 8.2 54.0 1.2 54.5 2.5 55.0 3.1 60.0 1.0 61.0 1.7 62.0 1.2 72.0 4.4 72.5 1.3 73.0 6.9 74.0 22.6 75.0 16.4 76.0 1.0 84.0 5.6 85.0 2.7 86.0 2.0 94.0 1.9 95.0 2.5 108.0 1.8 109.0 23.1 110.0 9.0 111.0 8.0 112.0 5.3 113.0 6.7 114.0 3.0 144.0 1.1 145.0 45.5 146.0 3.9 147.0 30.0 148.0 2.2 149.0 4.9 161.0 2.4 163.0 1.4 189.0 2.1 191.0 2.5 224.0 62.6 225.0 4.3 226.0 100.0 227.0 6.8 228.0 45.4 229.0 3.3 230.0 6.6
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H3 Br Cl2 0.05 ml : 0.5 ml CDCl3 1-bromo-2,4-dichlorobenzene Assign. Shift(ppm)
A 7.470 B 7.405 C 7.064
Hz ppm Int.
674.56 7.532 585 674.31 7.530 585 670.44 7.486 44 665.75 7.434 1000 664.38 7.419 796 662.19 7.394 892 658.38 7.352 56 657.06 7.337 41 637.31 7.117 681 634.88 7.089 579 631.69 7.054 48 631.25 7.049 48 628.75 7.021 456 626.31 6.994 391 622.75 6.954 30
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