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MassMS-IW-3512 3,3-dimethylpiperidine C7H15N (Mass of molecular ion: 113)
Source Temperature: 210 °C Sample Temperature: 160 °C Reservoir, 75 eV
15.0 1.0 27.0 6.2 28.0 9.8 29.0 10.6 30.0 24.9 39.0 9.8 40.0 1.9 41.0 20.5 42.0 10.5 43.0 12.1 44.0 100.0 45.0 4.3 53.0 2.9 54.0 1.9 55.0 11.6 56.0 31.5 57.0 51.7 58.0 2.6 67.0 3.3 68.0 2.7 69.0 3.7 70.0 15.5 71.0 3.0 80.0 1.0 81.0 1.3 82.0 2.9 83.0 2.0 84.0 4.9 85.0 1.6 96.0 2.4 97.0 1.0 98.0 17.3 99.0 1.2 112.0 10.0 113.0 37.1 114.0 3.1
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H15 N 0.05 ml : 0.5 ml CDCl3 3,3-dimethylpiperidine 
Assign. Shift(ppm)
A 2.720 B 2.468 C 2.28 D 1.489 E 1.336 F 0.906
Hz ppm Int.1092.53 2.734 82 1087.16 2.721 108 1081.54 2.707 86 986.33 2.468 321 912.48 2.284 71 607.42 1.520 31 601.32 1.505 64 595.58 1.491 99 590.21 1.477 76 584.23 1.462 47 539.55 1.351 111 533.33 1.335 115 527.34 1.320 77 363.16 0.909 645 362.30 0.907 1000 350.71 0.878 28
in CDCl3
liquid film
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