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网站主页CAS数据库列表 1190-09-6更多图谱(3-溴丙基)磷酸(1190-09-6)核磁图(13CNMR)

(3-溴丙基)磷酸

产品名称 (3-溴丙基)磷酸

CAS号1190-09-6

分子式C3H8BrO3P

分子量202.97

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  • Mass

    MS-IW-8621          
    (3-bromopropyl)phosphonic acid
    C3H8BrO3P           (Mass of molecular ion:    202)
    

       Source Temperature: 240 °C
       Sample Temperature: 210 °C
       Direct, 75 eV
    

          15.0       1.0
          17.0       3.3
          18.0      16.7
          19.0       1.3
          26.0       4.0
          27.0      11.7
          28.0      30.2
          29.0       6.6
          30.0       1.1
          31.0      15.0
          36.0       1.3
          37.0       1.8
          38.0       3.6
          39.0      21.7
          39.5       1.8
          40.0      10.7
          40.5       1.8
          41.0      58.5
          42.0      88.6
          43.0       4.8
          44.0       1.2
          45.0       5.0
          47.0      13.7
          48.0       2.4
          55.0       5.7
          57.0       9.6
          58.0      10.3
          63.0       1.3
          64.0       4.2
          65.0      39.7
          66.0       2.3
          78.0       2.7
          79.0      33.5
          80.0      95.1
          81.0      36.8
          82.0     100.0
          83.0       1.5
          91.0       2.3
          92.0      44.7
          93.0       3.6
          94.0      15.5
          96.0      89.7
          97.0       1.9
         103.0       1.8
         104.0       8.4
         105.0       5.1
         109.0       1.0
         121.0      45.7
         122.0      56.9
         123.0      13.3
         128.0       1.0
         168.0       1.3
         169.0       1.1
         185.0       1.4
    

400 MHz in DMSO-d6


  • 1H NMR 399.65 MHz
    C3 H8 Br O3 P 0.038 g : 0.5 ml DMSO-d6
    (3-bromopropyl)phosphonic acid
    ChemicalStructure
        Assign.     Shift(ppm)
    A 10.3 B 3.594 C 1.991 D 1.670

         Hz     ppm     Int.
    

       4106.29  10.275    246
       1443.48   3.612    486
       1436.77   3.596   1000
       1430.05   3.579    503
        816.65   2.044     70
        809.94   2.027    167
        804.29   2.013    171
        802.31   2.008    201
        800.93   2.005    158
        799.26   2.000    226
        798.19   1.998    220
        794.22   1.988    253
        792.69   1.984    212
        791.02   1.980    200
        787.81   1.972    193
        786.13   1.968     93
        782.78   1.959    180
        776.06   1.942     80
        683.90   1.712    301
        678.71   1.699    196
        675.81   1.692    264
        673.83   1.687    192
        668.18   1.672    263
        665.89   1.667    324
        660.71   1.654    197
        657.81   1.646    274
        655.82   1.641    191
        650.18   1.627    243
    

in DMSO-d6



KBr disc



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