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MS-NW-7036 bis(p-dimethylaminophenyl)methanol C17H22N2O (Mass of molecular ion: 270)
Source Temperature: 190 °C Sample Temperature: 170 °C Direct, 75 eV
15.0 3.0 18.0 3.4 27.0 1.2 28.0 1.6 39.0 4.1 41.0 1.5 42.0 15.6 43.0 1.6 44.0 4.2 50.0 2.6 51.0 4.7 52.0 1.9 53.0 1.2 63.0 3.6 64.0 1.4 65.0 3.5 66.0 2.1 68.0 1.0 75.0 1.9 76.0 3.5 77.0 13.9 78.0 7.1 79.0 6.9 80.0 1.5 89.0 1.6 90.0 2.2 91.0 6.2 92.0 2.4 93.0 1.5 96.5 1.0 102.0 1.0 103.0 1.7 103.5 1.5 104.0 8.1 105.0 8.9 106.0 4.5 107.0 7.5 110.0 1.0 115.0 1.8 117.0 1.6 118.0 12.4 118.5 1.6 119.0 8.6 119.5 1.0 120.0 18.9 121.0 13.5 122.0 38.4 123.0 3.9 125.0 1.0 126.0 7.4 126.5 2.9 127.0 2.6 132.0 5.5 133.0 2.6 134.0 10.7 135.0 4.1 139.0 1.1 140.0 1.1 148.0 52.6 149.0 7.7 150.0 11.3 151.0 2.1 152.0 2.6 153.0 1.8 163.0 1.0 164.0 1.1 165.0 7.7 166.0 3.1 167.0 1.4 179.0 1.0 180.0 1.0 181.0 1.0 192.0 1.3 193.0 1.6 194.0 2.8 195.0 1.2 196.0 1.3 197.0 1.1 208.0 3.0 209.0 3.2 210.0 10.1 211.0 1.9 221.0 2.4 223.0 2.0 224.0 5.3 225.0 1.6 226.0 1.6 237.0 18.8 238.0 5.3 239.0 3.0 240.0 1.7 251.0 3.0 252.0 1.7 253.0 100.0 254.0 46.1 255.0 6.8 267.0 3.1 268.0 12.3 269.0 13.2 270.0 67.1 271.0 13.4 272.0 1.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C17 H22 N2 O 0.042 g : 0.5 ml CDCl3 bis(p-dimethylaminophenyl)methanol Assign. Shift(ppm)
A 7.218 B 6.673 C 5.261 D 3.02 E 2.893
Hz ppm Int.
2889.28 7.230 138 2887.33 7.225 49 2882.32 7.213 51 2880.49 7.208 153 2878.91 7.204 43 2672.97 6.689 47 2670.65 6.683 166 2668.70 6.678 54 2666.02 6.671 21 2663.94 6.666 78 2661.87 6.661 151 2103.03 5.263 73 1208.74 3.025 136 1156.37 2.894 1000 1148.80 2.875 21
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